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GC/MS analysis report, sample AD23717, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23717 showing detection of unknown compounds on October 17, 2001.

NYC-WTC_000089171–000089184

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089183
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23717.D Vial: 13 Acq On : 15 Oct 2001 11:56 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 11.63 0.54 ug/1 49640 1,4-Dichlorobenzene-d4 11.76

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichloro^nzene-d4 150 C6C12D4 003855-82-1 50 2 Benzene-1,2/3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 Benzo [b] th^phene-4-ol 150 C8H6OS 003610-02-4 25 4 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 _______000148j253;18 10 Abundance / Scan 717 (11.627 min): 23717.D (-) m/z 149.90 100.00% 1!i0

5000 115 52 78 40 I 63 ,1 85 .................. I 11.20 11.40 11.60 11.80 12.00 ....... I' •......... 44^ m/z 151.90 61.65% ■n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-c)4 1!i0

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 115.00 34747%

TiZz-> 30 35 40 ‘ I ' ' ' ' r 50 60 UUn 70 80 90 100 110 120 130 I ’ ' * 'I 140' 150 4.^ 160 ^bundance #9592: Benzene-1,2,3,4-d4-, 5.6-dichloro- ■1!i0

115 11.20 11.40 11.60 11.80 12.00 5000 52 78 “raTz 78.05 19.72% (1 35 87 77^,r ' I' ' ' ' I ' ' ' ' I ' Ti/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 *\bundance #9645: Benzo[b]thiophene-4-ol 1!i0- -11.20 11.40 -11.60-11.80::i 2.00 "m/z 52.00 15.92% 121 5000

11® 96 ill 89 J II ' I ' ' ' ' I ' ' ' ' ) ' ' ' ' I ' n/i-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

23717.D NP091101.M Tue Oct 16 15:12:11 2001 Page . 5

NYC-WTC_000089183

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NYC-WTC_000089183Source: NYC Law Department, mirrored locally

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