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GCMS analysis results for sample AD24483, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24483 identifying unknown compounds on November 13, 2001.

NYC-WTC_000068763–000068777

Folder label: “GCMS Scan X 10/15/01 A 11/3/01

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Scanned page image, NYC-WTC_000068776
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0201\24483.D Vial: 22 Acq On : 3 Nov 2001 11:26 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1,4-Dichlorobenzene-d4 Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.59 ug/1 89230 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentatzive ID MW MolForm CAS# Qual

1 1,4-Dichloroben&ene-d4 150 C6C12D4 003855-82-1 95 2 Benzene-1,2,3y4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 53 3 Benzaldehyd^ 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 35 4 Benzoic aci. , 2,5-dimethyl- 150 C9H10O2 000610-72-0 9 Abundance / Scan 711 (11.573 min): 24483.D (-) m/z 149.90 100.00% 1$0

5000 115

52 78 ' I ' ' ' ' i ' ' ' ' i ■p’

11.20 11.40 11.60 11.80 12.00

■nfe-> .......... . 30 40 40 111 50 . ......... Up 60 70 80 ''' I ' 90 100 110 120 A 130 140 150 4^ 160 m/z 151.90 70.53% Abundance #9593:1,4-Dichloroben2ene-d4 1!i0

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 . 44.03% ,35, ........ 1,1............. n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5.6-dichloro- 1$0

115 11.20 11.40 11.60 11.80 12.00 5000 52 78 Wz 78.05 21.86%

35 87 1, .......... I ' r ' ' ' I ' '' ' I ' Ti/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- ' I ' ' ' ' I ' ' ' ' I ' ' 1$2 11.20 11.40 11.60 11.80 12.00 m/z 52.00 19.80% 106 5000 53 81

122 ' I'''' I'''' I 11111111111111 92 T-y+n-r-p- 136 I I Tlfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

24483.D NP103001.M Fri Nov 09 15:03:18 2001 Page 6

NYC-WTC_000068776

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NYC-WTC_000068776Source: NYC Law Department, mirrored locally

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