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← Document results/DEP Box 60/GCMS Scan X 10/22/01 An 11/8/01
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GC/MS calibration report, Nov 6 2001

Machine-extracted title · confidence 95%

Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.

NYC-WTC_000069271–000069279

Folder label: “GCMS Scan X 10/22/01 An 11/8/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\NOV2601\LB.D Vial: 8 Acq On : 26 Nov 2001 5:32 pm Operator: 209 GALOS Sample : 10/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 11.55 0.56 ug/1 192502 1,4-Dichlorobenzene-d4 11.68 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1 3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 4 Acenap^hylene______________________ 152 C12H8 000208-96-8 9 Abundance Scan 709 (11.554 min): LB.D {-) m/z 149.90 100.00% 1$0

5000 115

52 78 11.20 11.40 11.60 11.80 LXSrtk 87 94 m/z 151.90 . 66.62% ■n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593; 1,4-Dichlorobenzene-d4 1!i0

5000 115 78 11.20 11.40 11.60 11.80 52 m/z 114.90 . 37.58% 35 iife-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance i#9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1$0

115 11.20 11.40 11.60 11.80 5000 52 78 in/z 78.05 19.04%

35 I 'I ' ........ J,I.,. Ti/z-> 30 40 50 60 70 80 100 110 120 130 90 140 150 160 Abundance #66892; Benzaldehyde, 2-hydroxy-3-methoxy- 1$2 11.20 11.40 11.60 11.80 mTz 52.00 14.90% 106 5000 53 81

■n^-> ' I ' ' ' ' I ' ' ' ‘ I ' ' ' I ' ' ' ' I ' ' ' ' I '

30 40 50 60 70 80 92 n+r 122 A 136 I 90 100 110 120 130 140 150 160 I k 11.20 11.40 11.60 11.80

LB.D NP103001.M Tue Nov 27 09:37:10 2001 Page 2

NYC-WTC_000069278

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NYC-WTC_000069278Source: NYC Law Department, mirrored locally

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Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.

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