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← Document results/DEP Box 60/GCMS Scan X 10/22/01 An 11/8/01
Document / 9 pages

GC/MS calibration report, Nov 6 2001

Machine-extracted title · confidence 95%

Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.

NYC-WTC_000069271–000069279

Folder label: “GCMS Scan X 10/22/01 An 11/8/01”

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Scanned page image, NYC-WTC_000069277
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV2601\LB.D Vial: 8 Acq On ; 26 Nov 2001 5:32 pm Operator: 209 GALOS Sample : 10/22 Inst GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.67 1.57 ug/1 543035 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 T^tative ID MW MolForm CAS# Qual

1 2-Pentanope, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 38 2 3-Hydrojfi5^2-pentanone 102 C5H10O2 003142-66-3 9 3 Morpholine, 4-methyl- 101 C5H11N0 000109-02-4 9 4 Hyd:^.^ine, 1,1-bis (1-methylethyl) - 116 C6H16N2 000921-14-2 9 Abundance Scan 286 (7.671 min): LB.D (-) m/z 42.95 100.00% 4(3

59 5000

101 ' I ' ' ' ' I ' ' ' ' 7.40 7.60 7.80 8.00 37, I 70 77 8,3 I I I i'i I I ' I I I I I I I I I 126 m/z 59.05 53.97% 'I'’''I ' Tife-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #64275:2-Pentanone, 4-hydroxy-4-methyl- 40

5000 59 m/z 101.05 22.82% 15 31 101

L T-n-rXTy-TT-A-ftT-TT-p-Ht-r-r-p 83 I Tlfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1691:3-Hydroxy-2-pentanone 31 59

7.40> 7.60 7.80 8.00 5000 m/z 58.05 17.05% 45 15 I, .... ' I ' I] I y.J??, I..... . v/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1640: Morpholine, 4-methyl- 43 7.40 7.60 7.80 8.00 m/z 41.00 8.19%

5000

■nfe-> 10 15 I 20 27 T-pr-rr ^,■.'1.1....... 30 I 40 5.® I ' ' I ' ' I ■ I ' ■ ' ■ I' ■ ' • I ■ ■ "' I ■ * •. I""." I ■ ■' ' I".. ' I ■ 50 60 71 .I 70 80 90 101

100 110 120 130 7.40 L 7.60 7.80 8.00

LB.D NP103001.M Tue Nov 27 09:37:07 2001 Page 1

NYC-WTC_000069277

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NYC-WTC_000069277Source: NYC Law Department, mirrored locally

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