GC/MS analysis results for sample AD25072, Nov 28 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0901\25072.D Vial: 13 Acq On : 10 Nov 2001 12:07 am Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.68 2.40 ug/1 344355 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanon^ 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 50 2 2-PropanQZ, 2-methyl- 74 C4H1O0 000075-65-0 17 3 Morphol^e, 4-methyl- 101 C5H11N0 000109-02-4 9 4 3-Hydroxy-2-pentanone 102 C5H10O2 003142-66-3 9 Abundance Scan 287 (7.681 min): 25072.D {-) m/z 42.95 100.00% 40

59 5000

101 ' ' I ' ' ' ‘ I ' 83 7.40 7.60 7.80 8.00 53., ' I ' ■' I' I ' ' ' ' i r—T-i—r-r-|—1 ' I I ' ' ' I m/z 59.05 52.03% ■nZz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 40

5000 ' ' ' I ■ ' ’ r . . 59 7.40 7.60 7.80 8.00 m/z 101.05 22.41% 15 31 101 -r-r-T-r-rJ-r I I 83 , I ' I ' ' ' I ' ' ' ' I ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62572:2-Propanol. 2-methyl- 50

7.40 7.60 7.80 8.00 lililil ......... : 31 41

20 v/z-> 10 20 30 40 50 60 70 80 90 100110 Abundance #1640: Morpholine, 4-methyl- ' ' I ' ' ' ' I ' I ' . 40 7.40 7.60 7.80 8.00 m/z 41.05 7.17%

5000

101 15 71

■n/z-> ,,,i... y,. 10 20 30 40 50 56 60 ■ I'l • ' • I ■ ' ' I I ■ ' ■ > I I ■ ■ ■ I

70 80 90 100 110 7.40 7.60

25072.D NP103001.M Tue Nov 27 11:11:19 2001 Page 1

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