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GCMS analysis results for sample AD24476, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24476 conducted on November 14, 2001, identifying unknown compounds.

NYC-WTC_000068485–000068495

Folder label: “GCMS Scan X 10/12/01 An 11/3/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File ; C;\HPCHEM\1\DATA\NOV0201\24476.D Vial: 12 Acq On : 3 Nov 2001 1:44 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title ; 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.17 ug/1 194743 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 42 2 2-Propanol, 2-methyl- 74 C4H10O 000075-65-0 17 3 Morphol^e, 4-methyl- 101 C5H11NO 000109-02-4 9 4 Acetonjg 58 C3H6O 000067-64-1 9 Abundance Scan 288 (7.692 min): 24476.D (-) m/z 4^795 100.00% 4b fl 59 5000

101 7.40 7.60 7.80 8.00 69 83 ....................... I ' ' ' ' I ' ' ' ' I ■ I ' I I ' ■ ' ’ I m/z 59705 52.62%

L nfe-> 10 20 30 40 50 60 70 80 90 100 110 W)undance #64275: 2-Pentanone. 4-hydroxy-4-methyl- 43

5000 59 7.40 7.60 7.80 8.00 m/z 100.95 24.79% 15 31 I ryr-T-r-r-p I , ..I 83 I ' I I I . . I . I'l I'l . I 1 . I , , , , I I'l . . I , . , I I . , . , I ' 1 ' ■nA:-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62572: 2-Propanol. 2-methyl- 5b 7.40 7.60 7.80 8.00 in/z 58.05 ■ 17.79% 31 41

1,,,.^,.,,., , 2^, ,1, , 4 n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- 413 7.40 7.60 7.80 8.00 in/z 41.05 6.90%

5000 101 15 71 56 r+^ ' tLm-... I , , , , |l, , , , I Tlfe-> 10 20 30 40 50 60 70 80 90 100 110 7.^ 7.60 7.80' 8.00

24476.D NP103001.M Tue Nov 13 10:09:35 2001 Page 1

NYC-WTC_000068493

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NYC-WTC_000068493Source: NYC Law Department, mirrored locally

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