GCMS analysis results for sample AD26203, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC0401\26204.D vial: 69 Acq On : 4 Dec 2001 11:24 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 2.25 ug/1 646307 1,4-Dichlorobenzene-d4 11.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, hydroxy-4-methyl- 116 C6H12O2 000123-42-2 47 2 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 9 3 Butane / 58 C4H10 000106-97-8 9 4 5-Hexen-2-one 98 C6H10O 000109-49-9 9 Abundance Scan 288 (7.692 min): 26204. D (-) m/z 42.95 100.00% 43 59 5000

101 i ‘ ‘ । । . i i| । i |i i I I | i i i i 7.40 7.60 7.80 8.00

miz-> 38.1, 0+ TO—nn/Ln—nnn 10 20 30 40 +53+ 60 50 69 83 ' I ■ • • ■ i ■ ' ‘ 1 i 1 ' ■ ' i ■ ■ • 1 i 1 ■ ■ ■ i ■

70 80 90 100 110 m/z 59.05 49.66% Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 1*-010111i1111u— 59 7.40 7.60 7.80 8.00 m/z 100.95 20.55% 1— 15 31 + 1 1 150i Tt*t 60 - 3 — 1 101 8. — , .

miz-> 10 20 30 40 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- 43 ■ • 1 i • ■ ■ ■ i • ■ • ■ i ■ • ■ • i ■ ■ ■ ■ 7.40 7.60 7.80 8.00 5000 m/z 58.05 16.67% 101 15 71 27 56 ; ----- ' ' i 1 ' ' ' 1 ‘ ‘ ' I 1 ' ‘ ‘ I ‘ ‘ ‘ I ' ' ' ‘ I 1 1 ' ' 1 mz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #99: Butane — — r — 1 PPP P • 43 7.40 7.60 7.80 8.00 m/z 41.05 7.50% 5000 29

15 58 — — • 1 1 I ' — । । । ( । । । ।. ' I ' ' ' ‘ 1 m/z—> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

26204.D NP112601.M Tue Dec 04 16:02:08 2001 Page 1

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