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GCMS analysis results for sample AD26203, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD26203 with unidentified compounds detected.

NYC-WTC_000031118–000031128

Folder label: “GCMS X 11/2/01 A 12/1/01

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Scanned page image, NYC-WTC_000031127
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC0401\26204.D Vial: 69 Acq On : 4 Dec 2001 11:24 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise ' Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 11.57 0.58 ug/1 166302 1,4-Dichlorobenzene-d4 11.70 Hit# of Tentative ID 5 MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 72 2 Benzene-1,2,3 ,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 37 3 Biphenylene/ 152 C12H8 000259-79-0 9 4 Benzonitrile, 2-amino-5-chloro- 152 C7H5C1N2 005922-60-1 9 Abundance Scan 710 (11.566 min): 26204.D (-) m/z 149.90 100.00% 150

5000 115 52 78 TIOTeT ‘ T 1 1 1 1 । 1 11.20 11.40 11.60 11.80 40 il. . 1 r 87 .1 ।.... 11... 111 । Tt ‘ 111111... । — "11 ................................................................................................... m/z 151.90 . 60.82% miz-> 30 40 50 £0 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 TT T T 1 1 i • 78 1120 11.40 11.60 11.80 52 m/z 115.00 37.30% 35 87 L "II’ 11... t • ■ । • • ■ • । • 111111111' 111 —121000 mz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150

115 11.20 11.40 11.60 11.80 5000 52 78 m/z 78.05 20.23%

35 87 I ■ ■ i1 ■ ■ ■ I • ■ _................... , +11*P I > 111111.. । ■ i.. ।. । ■ ' i'1 ■ ■ i ■ ■ ' ’ I m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10447: Biphenylene —. । . . . . । . . . > । . . . . । k i . > । . 152 11.20 11.40 11.60 11.80 m/z 52.00 k 17.96% 5000

63 76

miz—> -7 - 30 40 50 1 60 100 110 120 130 140 150 160 70 80 90 98 128 * 11 '' ‘ f * ‘ * i • । । । । । . TT TTnanns 11.20 11.40 11.60 11.80

26204.D NP112601.M Tue Dec 04 16:02:11 2001 Page 2

NYC-WTC_000031127

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NYC-WTC_000031127Source: NYC Law Department, mirrored locally

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