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GCMS analysis results for sample AD24400, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting gas chromatography-mass spectrometry analysis of sample AD24400 conducted on November 5, 2001.

NYC-WTC_000068325–000068335

Folder label: “508 GCMS Scan X 10/11/01 An 11/2/01

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Scanned page image, NYC-WTC_000068334
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0201\24400.D Vial: 6 Acq On : 2 Nov 2001 7:55 pm Operator: 209 GALOS Sair^jle : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.52 ug/1 70757 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-DicMorobenzene-d4 150 C6C12D4 003855-82-1 72 2 Benzen^l,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 39 3 Biphe^lene 152 C12H8 000259-79-0 9 4 Acendphthylene__________________________ 152 C12H8 000208-96-8 9 Abundance Scan 711 (11.572 min): 24400.D (-) m/z 149.90 100.00% 1!O

5000 115

52 78 ‘ I ' * 11.20 11.40 11.60 11.80 12.00 38 ■ ■ I ■ ■ ■ • 11. I''' ■ 1 I '' I ■''' I' •'' I m/z 151.90 66.64% 30 40 50 60 70 80 90 100 110 120 130 140 IS) 160 Abundance #9593:1,4-Dichlorobenzene-d4 1$0

5000 115 1'1'^' 11*40 11.60' itap 'i2.oo 52 78 m/z 114.90 44.23%

Tife-> 30 35 40 .... I „,T, 50 60 70 80 90 ioo' iio' ,1 ....... w' '146 150 160 Abundance #959^ Benzene-1.2.3.4-d4-, 5.6-dichloro- 1$0 11'20 ’lt^' 11W '1’1.co '1'2'00 115 553 52 78 m/z 78.05 . 20.62%

87

Tife-> 30 35 f 40 50 60 70 I ' ' I ' ‘ ‘ ' I A I ‘ ‘ ‘ ‘ I 4^ 80 90 100 110 120 130 140 150 160 Abundance #67017: Biphenylene 11 ■' • • 1 ■ ■ • 1!i2 11.20 11.40 11.60 11.80 12.00 m/z 52.00 17734% 5000

63 76 126 97 -T]-! ( . . I . I . T 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

24400.D NP103001.M Mon Nov 05 12:20:52 2001 Page 2

NYC-WTC_000068334

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NYC-WTC_000068334Source: NYC Law Department, mirrored locally

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