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GCMS analysis results for sample AD24696, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24696 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068838–000068852

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24697.D Vial: 16 Acq On : 6 Nov 2001 2:35 am Operator: 209 GALOS San^jle : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* Peak Number 6 1,4-Dichlorobenzene-d4 Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.53 ug/1 88602 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 ’entative ID MW MolForm CAS# Qual 1 1,4-Dichl^obenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene2i,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 27 3 Biphen^ene 152 C12H8 000259-79-0 9 4 Acenaphthylene__________________________ 152 C12H8 000208-96-8 9 Abundance Scan 711 (11.575 min): 24697.D (-) m/z 149.90 100.00% 1!i0

5000 1 5 52 78 T 40 11.20 11.40 11.60 11.80 12.00 I'''' I m/z 151.90, 60.53% TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1!i0

5000 115 t 78 11.20 11.40 U.K) 11.80 12.00 52 m/z 115.00 35.20% 35 Tife-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5.6-diohloro- 1$0 ...... .JV.... 11 20 11,40 11.60 11.80 12.00 1 5 5000 52 78 m/z 78.05 18.97%

87

nfe-> 30 35 I 40 50 ‘ 1 ’ ’ ' * 1 ’ 60 70 I ' I' ''' 1' 80 90 100 110 A 120 130 140 150 160 Abundance #10447: Biphenylene 1G2 J 11.20 11.40 11.60 11.80 12.00 Wz 52.00 . 13.85% 5000

63 76 126 1..,.. . ...... 87 I' 98 lll^ 11^40 iVIbO 11'so 12'00 nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160

24697.D NP103001.M Tue Nov 13 12:05:45 2001 Page 6

NYC-WTC_000068851

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NYC-WTC_000068851Source: NYC Law Department, mirrored locally

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