GCMS analysis results, sample AD23844, Oct 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data Pile : C:\HPCHEM\1\DATA\OCT1701\23844.D Vial: 4 Acq On : 17 Oct 2001 4:13 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.53 ug/1 49761 1,4-Dichlorobenzene-d4 11.77 Hit# Of 5 fentative ID MW MolForm CAS# Qual

1 1,4-Dichl<^obenzene-d4 150 C6C12D4 003855-82-1 50 2 Benzene-1/2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 23 3 Biphenyl ^ne 152 C12H8 000259-79-0 9 4 Benzald) hyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 9 Abundance Scan 717 (11.621 min): 23844.D (-) m/z 149.90 100.00% 1!0

5000 115 52 78 40 1 11.y 11.40 11,60 11.80 12.00 m/z 151.90 59.53% m/z-> 30 40 50 60 70 8090 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobsn2ene-d4 1!l0

5000 115 I ■ • • • I • • • > fT I > ■ ■ ■ ■ I ■ ■

78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 37.49% 35 ■ Ti/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 ^bunctenca #9592: Benzene-1,2.3.4^, 5,6-<Jichlort>- 1!i0

115 11.a3 11.40 11.60 11.80 12.00 5000 52 78 “m/z 78.05 , 20.98%

nZz-> 30 35 I 40 50 60 70 87 I ' I' ■'' I' 80 90 100 110 A 120 130 I' ‘‘ I 140 -4— 150 160 Abundance #67017: Biphenylene 1112 11.^ 11.40 11.60 11.80 12.00 “mTz 52.00 17.08%

5000

63 76 T^rrnrr 126 97 -rVp- T-k I ‘ ‘ ‘ I ‘ ‘ ‘ ‘ I ' ' nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11,40 11.60 11.80 12.00

23844.D NP101901.M Tue Oct 23 12:45:08 2001 Page 5

NYC-WTC_000067451