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GC/MS analysis results for sample AD23345, Oct 16 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23345 conducted on October 16, 2001.

NYC-WTC_000088556–000088584

Folder label: “GC/MS Scan 9/26/01

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Scanned page image, NYC-WTC_000088567
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23345.D Vial; 17 Acq On : 10 Oct 2001 4:57 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. 11.63 0.56 ug/1 53956 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 TXntative ID MW MolForm CAS# Qual 1 1,4-Dichlg/bbenzene-d4 150 C6C12D4 003855-82-1 50 2 Benzene- l<2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 32 3 Trimethyd thioborate 152 C3H9BS3 000997-49-9 9 . 4 Biphen^ ene 152 C12H8 000259-79-0 9 Abundance ' Scan 717 (11.625 min): 23345.D (-) m7z‘T^4y790 100.00% 1!i0

5000 115 52 78 40 11.20 11.40 11.60 11.80 12.00 4^ m/z 151.90 63.38% nfe-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 #9593:1,4-Dichlorobenzene-d4 A I'iO

5000- 115 y-r-T-T-r-^-r-r-r-r^^

78 11.20 11.40 11.60 11.80 12.00 52 m/z 115.00 34.59%

n/z-> 10 20 30 35 40 A 50 60 70 80 90 100 110 120 130 140 150 160 4^ Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- I'iO I ' ' ' ' I 115 11.20 11.40 11.60 11.80 12.00 5000 52 78 "mTz 78.05 17774%

87

Ti/z-> 10 20 30 35 I 40 50 60 70 80 I A 90 100 110 120 130 140 150 160 Abundance #10058: Trimethyl thioborate 152 11.20 11.40 11.60 11.80 12.00 “mTz 52.00 16.91% 47 137 5000 106

15 61 87 I ' I' ' ' ' I ' ' ' ' I ' ' ' ' I' I TpT-r*T-p-rTT-p- 1'"' 11 • • ■ 1 > > I > I ■ • • ‘ I T-r-j-r-r n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

23345.D NP091101.M Thu Oct 11 13:09:49 2001 Page 5

NYC-WTC_000088567

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NYC-WTC_000088567Source: NYC Law Department, mirrored locally

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