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GCMS analysis results for sample AD24640, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24640 with detection of unknown compounds on November 13, 2001.

NYC-WTC_000068659–000068671

Folder label: “508 Scan X 10/16/01 A 11/5/01

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Scanned page image, NYC-WTC_000068670
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV0 501\24640.D Vial: 13 Acq On 5 Nov 2001 11:40 pm Operator: 209 GALOS Sample gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.52 ug/1 84180 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForrn CAS# Qual

1 1,4-Dichloj;j0t5enzene-d4 150 C6C12D4 003855-82-1 64 2 Benzene;;ar72,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 33 3 Trimi tliyl thioborate 152 C3H9BS3 000997-49-9 9 4 Van!' lin 152 C8H8O3 000121-33-5 9 Abundance Scan 712 (11.579 min); 24640.D (-) m/z 149.90 100.00% 1ii0 ft 5000 115 52 "8 11.20 11.40 11.60 11.80 12.00 40 87 ,1 '' I'''' r ' ‘' I ‘' I' ' 'I ' I ' ' ' ' I ' ‘ ' I 4^ m/z 151.90 61.97% mZz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593; 1,4-Dichlorobenzene-d4 1!i0

5000 115 ' I ' ' ' ' I ' ' ' ' ' I ' ' ' ‘ I ' 78 11 20 11,40 11,60 11,80 12.00 52 m/z 114.90 2^747%

m/z-> 35 ' I'''' I'''' I'''' I'''' r 10 20 30 40 50 60 70 80 A 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1.2,3,4-d4-. 5,6-dichloro- 150

115 11 20 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 . 18.37%

35 87

m*::>10 20 I 30 40 50 ' I" " I' 60 70 I I' ‘' I " " I 80 A 90 100 110 120 130 140 150 160 ym-rp-m-

Abundance #10058: Trimethyl thioborate 152 11 20 11.40 11.60 11.80 12.00 m/z 75790 12.46% 47 137 5000 106

15 61 87 ,,, I................. I I I I rrp i . . I I I I I I I ITT) . 72 I " I " " I'''' I " " I' ' I ■" ‘ I" " I ■' I ’ I" " I \ mZz-> 10 20 30 40 50 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

24640.D NP103001.M Fri Nov 09 12:25:43 2001 Page 4

NYC-WTC_000068670

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NYC-WTC_000068670Source: NYC Law Department, mirrored locally

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