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GCMS analysis results for sample AD24293, Nov 7 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24293 conducted on November 7, 2001, noting unknown compounds.

NYC-WTC_000068213–000068223

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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Scanned page image, NYC-WTC_000068222
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0601\24293.D Vial: 1 Acq On : 6 Nov 2001 12:47 pm Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.53 ug/1 95179 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 T/ntative ID MW MolForm CAS# Qual 1 l,4-Dichlo3?6benzene-d4 150 C6C12D4 003855-82-1 50 2 Benzene-l/z,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 1,2,5-Tythiepane 152 C4H8S3 006576-93-8 10 4 Acenapl^chylene 152 C12H8 000208-96-8 9 ^bundance 7 Scan 711 (11.575 min): 24293.D (-) m/z 149.90 100.00% 1$0 fl

5000 115 52 78 40 11.20 11.40 11.60 11.80 12.00 I.. 63 ,|| 87 •nfe-> 30 '' I ‘ • 'T'’* 40 50 60 70 80 rX 90 100 110 120 130 140 150 160 m/z 151.90 68.48% Abundance #^3:1,4-Dichlorobenzene<j4 1$0

5000 115 1'1 '1'1 ^40' 'iw IZOD 52 78 m/z 114.90 . 37.86% 35 ■TTym- ■ I ■ ■ ■' I ' ‘ ‘ I' nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 ^bundance #9592: Benzene-1,2,3,4-<i4-, 5.6-dichtoro- 1$0 T ' ' ‘ I ' 115 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z77.95 16.87%

87 TiZz-> 35 I "30" ' 40''' 93 ' I' ‘' I' 60 70 80 I ' I' ''' 1' 90 100 110 120 A 130 140 150 160 Abundance #10068:1,2.5-Trithiepane ■-I ‘ ' I ' It 12 11.20 11.40 11.60 11.80 12.00 m/z 52.00 15.68%

5000 60 87 45 78 106 124

Tlfe-> 30 40 50 60 70 4^ JXX I'''' I'''' r '' ‘ I 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

24293.D NP103001.M Wed Nov 07 09:08:13 2001 Page 2

NYC-WTC_000068222

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NYC-WTC_000068222Source: NYC Law Department, mirrored locally

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