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GCMS analysis results for sample AD26164, Dec 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD26164 performed on December 3, 2001, noting other unknown compounds.

NYC-WTC_000031063–000031075

Folder label: “GCMS X 11/2/01 A 12/1/01

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Scanned page image, NYC-WTC_000031073
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3001\26164.D Vial: 61 Acq On 1 Dec 2001 1:27 am Operator: 209 GALOS Sample 11/2 gc/ms Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.59 ug/1 132915 1,4-Dichlorobenzene-d4 11.70 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorobenizene-d4 150 C6C12D4 003855-82-1 97 2 Benzene-1,2,3 ,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 53 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 35 4 Biphenylene 152 C12H8 000259-79-0 9 Abundance Scan 710 (11.559 min): 26164.D (-) m/z 149.90 100.00% 150

5000 115 78 ......... ...... ...... 52 ’d- TTTI 1 1.d i r-t-—-I T [ T 11.20 11.40 11.60 11.80 —3 38 tmm T । *•* <i‘ i • * * * 87 n 11 i1111111।11i111: it 11 207 m/z 151.90 67.47% mlz-> 30 40 50 60 70 80 SO 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 78 11.20 11.40 11.60 11.80 52 m/z 114.90 43.39% 35 87 U’II111T t rp-rr ■ ■ i ■ • ■ ■ i ■ ■ ■' i -rrrp-rrq-rT —lmm 1................. miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #9592: Benzene-1,2,3,4-d4-,5,6-dichloro- 150

115 11.20 11.40 11.60 11.80 ‘ ' 5000 52 78 m/z 78.05 24.56%

35 87 I -rrrp-rrrp-r ----- " i'"' i • ■' ■ i miz-> 30 40 50 60 70 80 90 100110120130140150160170180190200 210 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 1$2 11.20 11.40 11.60 11.80 ' m/z 52.00 22.03% 106 5000 53 81

122

m/z—> 1’1—221112111 T-STi-m-rp-i-.-rp-,- 136 TTTEmni XA4 I 11110 i j n > ipTrrpn-rrprrrpTT 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 1120 1140 11.60 1180 '

26164.D NP112601.M Mon Dec 03 12:20:17 2001 Page 3

NYC-WTC_000031073

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NYC-WTC_000031073Source: NYC Law Department, mirrored locally

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