GCMS analysis results for sample AD26164, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3001\26164.D Vial: 61 Acq On 1 Dec 2001 1:27 am Operator: 209 GALOS Sample 11/2 gc/ms Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Nonane, 4-methyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 35.58 0.91 ug/1 140115 Perylene-dl2 37.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Nonane, 4-methyl- 142 C10H22 017301-94-9 14 2 Pyridine, 4-[4-methoxyphenyl] - 185 C12H11NO 000000-00-0 12 3 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 12 4 Octane, ethyl- 142 C10H22 015869-86-0 9 Abundance Scan 3327 (35.584, min): 26164.D (-) m/z 185.10 100.00% 185

57 5000 43 71 112 84 98 ------- 35.20 35.40 35.60 35.80 36.00 m 1,203 125 143 166 297 miz-> 20 —t HH—r ।j m/z L TI-1Ii T[I । । j । 116t 40 as 80 100 120 io 160 180 200 220 240 260 280 300 । t । । । । i i i t । । । । । । । । । i । i i ri । i i i i । । 57.0.0 58.20% Abundance #8099: Nonane, 4-methyl- 57

5000 70 । T Mr 35 20 35.40 35.60 35.80 36.00 98 m/z71.10 37.28% xu 27 42

L 85 112 142 IT —110111]u———OOIOIIT-n—uu——T——pdoog1 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #19196: Pyridine, 4-[4-methoxyphenyl}- 185 T 4 TT 35.20 35.40 35.60 35.80 36.00 5000 m/z70. 10 37.15%

L 142 115 170 63 89 ....... 76 1 pin । rr ri pn T’1’’1111 ----- — - m/z—> 20 40 60 80 100 120 140 160180 200 220 240 260 280 300 Abundance #32687: Propanedioic acid, hexyl-, diethyl ester ■ i 1 ' ' ‘ i ' ‘ ‘ * i • 57 35.20 35.40 35.60 35.80 36.00 70 m/z 112.10 33.38% ( 5000 83 112

42

m/z—> —l 20 40 i *' “ I 60 80 98 11111 1 199 217 ' i ■ ' • ■ i ■ ■ ‘ ■ i • • • ■ i • ■ • ■ i ' ■ • i ■ ■ ■ ■ i ■ ■ 1 1 I 1 ' 1 1 I 1 1 1 1 I 1 100 120 140 160 180 200 220 240 260 280 300 1 i । i i t i । i : » : । : i i i j : » J” T | : 35.20 35.40 35.60 35.80 36.00

26164.D NP112601.M Mon Dec 03 12:20:19 2001 Page 4

NYC-WTC_000031074