GCMS analysis results for sample AD26320, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3 001\26320.D Vial: 19 Acq On 1 Dec 2001 4:35 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Decanedioic acid, bis(2-ethylh Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 35.71 2.33 ng/uL 1010790 Perylene-d12 37.29 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3 Q 2 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 35 3 Octane, l,l'-oxybis- 242 C16H340 000629-82-3 14 4 Octane, l,l'-oxybis- 242 C16H34O 000629-82-3 12 Abundance Scan 3366 (35.710 min): 26320.D (-) ~Tm/z 185.10 100.00% 185 57

5000- 70 _____________ ) ( 43 112 83 98 * ' i 4 1 • • i 1 • ‘ • i ' ‘ 1 • I ‘ * * * i । I 125 143 166 | 203 35.40 35.60 35.80 36.00 297 315 253 268 ′ i W । T —r । 4 -|' i11' । 4 । , A A । . । » » । । । i • । r » । i [ । । » • । 1101 m/z 57.10 69.65% mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320

.J Abundance #55661: Decanedioic acid, bis(2-ethylhexy!) ester 185

5000 57 ■ • i • > TTT 71 112 35.40 35.60 35.80 36.00 m/z 70.05 46.19% 84 98 125 143 166 298 • ■ i ■ ■ •11 • — F— 11 — — 203 Y — — 316 9”, ■<nfz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #32687: Propanedioic acid, hexyl-, diethyl ester 57 70 35.40 35.60 35.80 36.00 ‘'1 5000 m/z 71.05 42.89%

1 83 112

42 98

miz-> 40 LX 60 80 100 120 140 160 180 200 220 240 260 280 300 320 11 • ■11 1 • • i ■ • T!—T0101010111000011000upang 199 217

Abundance #32426: Octane, 1,1-oxybis- ■ ' i 1 ■ • 1 i ’ ‘ ■ ‘ i ■ ■ ■ 1 i ' ‘ ' i 57 71 35.40 35.60 35.80 36.00 m/z 43.10 37.27% 5000 84 42

‘ ‘ I * * 197 12 131............ I’ KI i | i t i | i » T i | 1 1 : i | i i I : | i 1 i i j ! i i i | i 1 i i | i 1 ( r ] i i » i । i : i i । i < i 1 | I 1 J t | J 2 = TTTM m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 35.40 35.60 35.80 36.00

26320.D NP112701.M Tue Dec 04 10:13:07 2001 Page 5

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