GCMS analysis results for sample AD29788, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD29788 conducted on January 9, 2002, by the DEP.

NYC-WTC_000037156–000037165

Folder label: “GCMS X 12/10/01 A 12/15/01”

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Data File : C:\HPCHEM\1\DATA\DEC1401\29788.D Vial: 18 Acq On 15 Dec 2001 7:07 pm Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Decanedioic acid, bis(2-ethylh Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

35.57 1.84 ug/1 379525 ' Perylene-dl2 37.10

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic acid, bis (2-ethylhexyl) 426 C26H50O4 000122-62-3 64 2 2-Undecene, 4,5-dimethyl-, [R@,S@-( 182 C13H26 055170-93-9 17 3 Octane, 1,1 ' -oxybis- 242 C16H340 000629-82-3 10 4 Octa: , 2,5-dimethyl- 142 C10H22 _______ 015869-89-3 10 'Abundance Scan 3325 (35.571 min): 29788.D (-) m/ z 185.10 100.00% I 185 57 5000 70 43 112 ....................... 83 98

miz-> 40 JU—L T 60 80 125 143 166 'I ' ' ' 'I 203 1 i 100 120 140 160 180 200 220 240 260 280 300 320 268281 297 315 -|-n-n-p IUIuuurr • । ■ ■ ■ ■ । 35.20 m/ z 35.40 35.60 35.80 36.00 57.00 63.17% Abundance #55661: Decanedioic acid, bis(2-ethylhexyl) ester 185

5000 57 ‘d" r 11 l 71 112 35.20 35.40 35.60 35.80 36.00 84 98 m/z 70. ...... ! 125 143 166 298 316 1 1 | 203 i1 1' • i ■' ।' • ■ ■ । m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #18485: 2-Undecene, 4,5-dimethyl-, [[email protected]@-(Z)]- 43 57 1 i ■ • ■ ■ i ■ ' T 71 35.20 35.40 35.60 35.80 36.00 5000- m/ Z 71.00 40.21% 115 84 98 ' 140 t 182 > > i ■ ■ ■ ■ । ■ ' I ’ ' 1 .-r-rrTrmyrrTT T‘It11‘tIIr miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #32426: Octane, 1,1‘-oxybis- T11.......... 57 71 35.20 35.40 35.60 35.80 36.00 m/z 55.00 35.63% 5000- 84 42

m/z—> TIIIT TIT 1 40 60 I.971112 131____________ ____ ________________ T‘ET"EEI1-TTTT01T10TIECOIETTTTT1T ‘TTTTIT 80 100 120 140 160 180 200 220 240 260 280 300 320 == e 35.20 35.40 35.60 35.80 36.00

29788.D GCMS1126.M Fri Dec 28 13:23:53 2001 Page 2

NYC-WTC_000037164

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GCMS analysis results for sample AD29790, Jan 2002 · Box DEP Box 22

NYC-WTC_000037146

Laboratory report documenting GCMS analysis of sample AD29790 conducted on January 9, 2002, by the DEP.

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