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GCMS analysis results for sample AD30985, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.

NYC-WTC_000018262–000018285

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30985.D Vial: 39 Acq On 2 Jan 2002 1:45 am Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Decanedioic acid, bis(2-ethylh Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

35.58 25.47 ug/1 4400830 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3 87 2 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 35 3 [1,11-Biphenyl]-4-ol, 3-amino- 185 C12H11NO 001134-36-7 22 4 4-Undecanol, 7-ethyl-2-methyl- 214 C14H30O 000103-20-8 16 Abundance Scan 3326 (35.576 min): 30985.D (-) m/z 185.10 100.00% 185

miz-> 5000 57

83

34.414.4.142343466, 112

203221240 268 297315 MIUumumumumuaa) 40 60 80 100120140160180200220240260280300320340360380400420 355 401 429 2 35.20 35.40 35.60 35.80 36.00 m/ Z 57.00 62.86% 1 ' i •

Abundance

i 5000 #55661: Decanedioic acid, bis(2-ethylhexy!) ester

57

83 112

143 166 I i TTTTp 185

203 298316 m/z J 35.20 35.40 35.60 35.80 36.00 70.10 42.91% ’ **}’* T’TIII"T m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 'Abundance #32687: Propanedicic acid, hexyl- diethyl ester 57 1 i ■ ■ ■ ■ i ■ • 1 ■ i ‘ ‘ • 1 i ' 1 • ' i ' 35.20 35.40 35.60 35.80 36.00 5000 m/z 71. ,0 39.25% 83 112

i il 199217 T—_umu"———ne=m—nanm2nmn—m—“———B2““Pp miz-> 40 60 80 100120140160160200220240260280300320340360380400420 Abundance #19199: [1,r-BiphenyI]-4-ol, 3-amino- 185 35.20 35.40 35.60 35.80 36*00 m/z 43.00 34.33% 5000 156

m/z-> „8pL, I’uuu—mnuROTIII) 40 60 80 100120140160180200220240260280300320340360380400420 i j । । i । r i । iTrr| 1’11 I 35.20 35.40 35.60 35.80 36.00

30985.D GCMS1126.M Wed Jan 23 08:58:06 2002 Page 14

NYC-WTC_000018282

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NYC-WTC_000018282Source: NYC Law Department, mirrored locally

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