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GCMS analysis results for sample AD30984, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD30984 conducted on January 25, 2002.

NYC-WTC_000018248–000018261

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018260
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30984.D Vial: 38 Acq On 2 Jan 2002 12:47 am Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Decanedioic acid, bis(2-ethylh Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

35.60 238.32 ug/1 46074200 Perylene-dl2 37.12

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3 @2 2 [1,11-Biphenyl]-4-ol, 3-amino- 185 C12H11NO» 001134-36-7 27 3 Pyridine, 4-[4-methoxyphenyl]- 185 C12H11NO> 000000-00-0 12 4 Propanedioic acid, hexyl-, diethyl 244 C13H2404: 005398-10-7 12 (Abundance Scan 3328 (35.599 mln): 30984.D (-) m/z 185.10 100.00% 185

57 5000 । 112

m/z-> 0- Abundance 3 nnfmhmmm ] 83 1 1 | J I If3 166 203221240 268 297315 340 369 397 427 i. |i,.. ।..., 1,,, 11. i।..,n।..,.|....1111,1111111111111111 40 60 80 100120140160180200220240260280300320340360380400420 #55661: Decanedioic acid, bis(2-ethylhexy!) ester m/z "T 1**‘I** • ■ i ■ ■ 35.20 35.40 35.60 35.80 36.00

185

5000 57 T T T T T 1 112 35.20 35.40 35.60 35.80 36.00 m/z 70.10 38.76% Tm-p-r ’ 83.1149 166 Tmp] 203 *——44480444*1*84418*881 298316 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #19199: [1,1-Biphenyi]-4-ol, 3-amino- 185

35.20 35.40 35.60 35.80 36.00 5000 m/z 71.05 36.03% 156 128

m/z-> 40 60 80 100120140160180 200 220 240 260280 300 320 340 360 380 400 420 ‘ Abundance #19197: Pyridine, 4-[4-methoxyphenyl]- 185 35.20 35.40 35.60 35.80 36.00 m/z 112.10 32.86% 5000 115 142 63 I89 m/z-> l ,| 40 60 80 100 120140160180 200 220 240 260 280 300 320 340 360 380 400 420 ' 35.20 35.40 35.60 35.80 36.00

30984.D GCMS1126.M Wed Jan 23 08:53:45 2002 Page 6

NYC-WTC_000018260

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NYC-WTC_000018260Source: NYC Law Department, mirrored locally

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