Laboratory report documenting GCMS analysis of sample AD30984 conducted on January 25, 2002.
NYC-WTC_000018248–000018261Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search compound. Report
Data File C:\HPCHEM\1\DATA\DEC3101\30984.D Vial: 38 Acq On 2 Jan 2002 12:47 am Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *************************************************************** * ***** Peak Number 5 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
20.28 1.84 ug/1 756475 Acenaphthene-dl 0 20.56
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 40 2 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 36 3 4-Al ino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 27 4 Octi decanoic acid, 2-[(trimethylsil 386 C22H46O3Si 056196-58-8 10 Abundance Scan 1659 (20.277 mtn): 30984.D (-) m/z 72.9,5 100.00% 73
5000 147 281 327 * • *! * * • • I* * ‘ • 1 • * 4*8 *
m/z-> 45 — 50 100 —11—+ 150 200 250 +4350 383400415. 450 500 550 m/z 147.00 300 1191 251 Pin r221Pfim , .20.00 20.20 20.40 20.60 33.78% Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 281 5000 i j k। n IA’ll I’I" jn t ITT i' i'' i t 20.00 20.20 20.40 20.60 369 m/z 281.00 31.78% 207 249, 338 I * > • t l • miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503; 3-isopropoxy-1.1.1.7.7.7-hexamethyl-3,5,5-tris(trim 73 20.00 20*20 20.40 20.60 5000 m/z 326.90 12.63% 147 221 281 327 415 I 519 561 ‘ 1 I 1 • ■ ■ i ' ' miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #48317:4-Amino-5-imidazole carboxamide, tris(trimethylsily • ‘ i 1 ‘ ■ 11 ' ' r i ■ ■ • ■ i ■ ■ 73 20.00 20.20 20.40 20.60 m/z 282.00 8.98% 327 5000 237 45 147 I 172 • 1 i ' • ■ 1 i ■ ■ ■ ■ i ■ • ■ • i 212 • L , I l ) • • • • l • •n . | . . * . | * . . . | . I i 1 r I I I m/z-> 50 100 150 200 250 300 350 400 450 500 550 20.00 20.20 20.40 20.60
30984.D GCMS1126.M Wed Jan 23 08:53:40 2002 Page 5
NYC-WTC_000018259
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NYC-WTC_000018093
Automated laboratory log recording GCMS analysis of sample AD30694 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018142
Automated laboratory log recording GCMS analysis of sample AD30711 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018650
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30906 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017478
Laboratory report documenting GCMS analysis of sample AD31075 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016783
GCMS analysis of environmental sample AD30118 conducted January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036815
GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036842
GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036542
Laboratory commentary noting detection of bis(2-Ethylhexyl)phthalate in sample AD29520 and blank on January 25, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder