Laboratory report documenting GCMS analysis of sample AD31018 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
NYC-WTC_000017380–000017404Folder label: “GCMS X 12/20/01 A 1/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
'Data File C:\HPCHEM\1\DATA\JAN0 802\31018.D Vial: 14 Acq On 9 Jan 2002 2:01 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
20.13 4.75 ug/1 1428680 Acenaphthene-dl0 20.39
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane,1, 1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 47 2 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 38 3 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 12 4 Octadecanoic acid, 2-[(trimethylsil 386 C22H46O3Si 056196-58-8 9 Abundance “ T.............. Scan 1643 (20.128 min): 31018.D (-) m/z 72.95 100.00% 73
5000 147 281 327 ri221Pi’251ri A,-| r 1 355,383 415... . 45 .. 19.80 20.00 20.20 20.40 — 117 #i*h 11" 191 m/z 147.00 36.30% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 281 5000 .... . .. 0 19.80 20.00 20.20 20.40 369 m/z 281.0,0 34.76% 207 249, I. I 338 I m/z->__ 50 100 150 200 250 ' 300 ' 350 ' 400 ' 450 ' 500 ' 550 ' Abundance 73
19.80 20.00 20.20 20.40 ' ‘ ' 5000 m/z 326.9.0 13.89% 147 221 281 327 415 519 561 m/z-> 50 100 150 200 ' 250 ‘ ' 300 ‘ ' 350 ' 400 ‘ ' 450 ' ' 500 ‘ ' 550 ‘ Abundance #48317:4-Amino-5-imidazole carboxamide, tris(trimethylsily 73 19.80 20.00 20.20 20.40 ' m/z 282.00 9.41% 327 5000 237 45 1 I ‘ ‘ i ' ‘ । 172 212 t' ik। ■ ■ ■ 147 ‘ i ‘ ‘ ' ■ i ■ ' ■ ■ i I I.......... * | » * T * | * * I I | * * * I | * । » । 1 1 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 19.80 20.00 20^20 20.40 ‘ '
31018.D GCMS0103.M Wed Jan 09 12:07:55 2002 Page 6
NYC-WTC_000017392
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NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017405
Laboratory report documenting GCMS analysis of sample AD31074 conducted on January 18, 2002, noting no unusual compounds were detected.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000017329
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Filed in the same folder
NYC-WTC_000017330
Fragmented page from a laboratory method document regarding extraction and analysis procedures for GCMS testing.
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NYC-WTC_000017334
Laboratory report documenting GCMS calibration analysis of sample AD31017 conducted on January 8, 2002, listing concentrations of various organic compounds.
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NYC-WTC_000017338
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31017 performed on January 18, 2002.
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NYC-WTC_000017344
Laboratory report listing detection limits for numerous organic compounds in a GCMS blank sample analyzed on January 10, 2002.
Filed in the same folder