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GCMS analysis results for sample AD31018, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD31018 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.

NYC-WTC_000017380–000017404

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document

Library Search Compound Report ‘Data File C:\HPCHEM\1\DATA\JAN0 802\31018.D Vial: 14 Acq On 9 Jan 2002 2:01 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Propanone, 1-(1-methylethoxy Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 18.01 0.83 ug/1 251046 Acenaphthene-dl0 20.39 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1- (1-methylethoxy) - 2 Butane / 3 2-Propenenitrile, 3-(acetyloxy)- 116 C6H12O2 58 C4H10 111 C5H5NO2 4 2-Butanol, 2-nitroso-, acetate (est 145 C6H11NO3 Abundance

5000 I 43 57 Scan 1412 (18.007 mln): 31018.D (-)

73 111 m/z I 042781-12-4 12 000106-97-8 9 014268-54-3 9 013880-90-5 9 100.00%

Tuna * TJ I ‘ 95 ' I ' TmPr

127 146 17.60 17.80 18.00 18.20 1840 mmmml 1 . . 85 *wnnpmn"p 4 TT —mE——g——a—p—nmmp 201 m/z 57.00 71.01% m/z-> ... 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 Abundance #3286: 2-Propanone, 1-(1-methylethoxy)- 43

5000 /ka r 17.60 17.80 18.00 18.20 18.40 27 58 73 m/z 73.00 58.35% 1.... .,l!i....... 1............................................................................ m/z- _ 10 20 30 40 50 60 70 80 90 100 110120130140150160170180190200 Abundance 43 —IPUPImfT 17.60 17.80 18.00 18.20 18.40 5000 29 m/z 111.10 45.02% 58 15 pTrTpTTTpTTrpTTTTTTTTpTTTpTTTpTTTTTTTTpTTTpTTTTTTTTpTTrp-^^ 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 Abundance #2407: 2-Propenenitrile, 3-(acetyloxy)- 43 111 17.60 17.80 18.00 18.20 18.40 m/z 69.10 29.59% 5000

15 77 TH 52 I 94 ll nij11111।।j।j।( m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 17.60 17.80 18.00 18.20 18.40

31018.D GCMS0103.M Wed Jan 09 12:07:50 2002 Page 5

NYC-WTC_000017391

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NYC-WTC_000017391Source: NYC Law Department, mirrored locally

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