GCMS calibration table for TCLP analysis, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0 802\28327.D Vial: 5 Acq On 8 Jan 2002 4:16 pm Operator: 209 GALOS Sample 508 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Propanone, 1-(1-methylethoxy Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

18.00 0.95 ug/1 476234 Acenaphthene-dl0 20.40

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone,/1- (1-methylethoxy) - 116 C6H12O2 042781-12-4 17 2 2-Butanol, /-nitroso-, acetate (est 145 C6H11NO3 013880-90-5 9 3 Pentane, 2,3,4-trimethyl- 114 C8H18 000565-75-3 9 4 Propanoic/acid, 1-methylethyl ester 116 C6H12O2 _____ 000637-78-5 9 Abundance ' Scan 1411 (18.001 min): 28327.D (-) m/z 43.05. 100.00% 43 57 73 5000 111 95 TeT L........._ ।11111'11111'

mz-> mm l +orr TT . 85 HTTTTTT , +127 146 201 CITTTTTTTTTTTTTTT :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 17.60 m/z 17.80 57.00 18.00 18.20 18.40 68.08% Abundancer #3286: 2-Propanone, 1-(1-methylethoxy)- 43

----- —.. 1 — ■ 5000 i T 1 TT T1 17.60 17.80 18.00 18.20 18.40 27 m/z 73.00 57.23% II, I ll „ 58 73 l l____ I______________ __________ 'i p ■ TTT i it pl 1111TTTTUT TIOgum TTTTTTYTTTTTTTTTTTTOTT 111 p i up, 11 pin । TTTTT miz-> :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance $8505: 2 Butanol, 2-nitroso-, acetate (ester) 43 --PPP TTT1 17.60 17.80 18.00 18.20 18.40 5000 m/z 111.10 41.66% 73 TT 27 56 i 86 115 145 TTTTT i" ■ ■ i ■" ■ i ■1" i"'' i" i 1 ,ii । TTTTTTTTT ... p i. i p ., i p i irp i n p 111 p i n । m/z- :20 30 40 50 6070 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance! #3100: Pentane, 2,3,4-trimethyl- । ' ' ■ ' । 1 1 •1 । ■' ।'1'' i'1 | 43 17.60 17.80 18.00 18.20 18.40 m/ Z 69 .10 27.14% 71 5000-

27 55

I . 114 11 > 1111111.। (I..p.T.TTTTTgmg ।r,iiTTTTTT rmTT .. ph. 11< ।h ।.।h।.... ।.. ।.। 3,, J V, . , miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 17.60 17.80 18.00 18.20 18.40

28327.D GCMS1126.M Wed Jan 09 09:14:57 2002 Page 4

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