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GC/MS calibration data for sample 28322, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018492–000018518

Folder label: “GCMS X 12/18/01 A 12/30/01

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\28322.D Vial: 62 Acq On : 30 Dec 2001 7:56 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 2-Propanone, 1-(1-methylethoxy Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T.

18.15 0.88 ug/1 438511 Acenaphthene-dl0 20.56 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1-(1-methylethoxy)- 116 C6H1202 042781-12-4 25 2 2-Propenenitrile, 3-(acetyloxy)- 111 C5H5NO2 014268-54-3 16 3 Pentane, 2,3,4-trimethyl- 114 C8H18 000565-75-3 10 4 2-Butanol, 2-nitroso-, acetate (est 145 C6H11NO3 013880-90-5 9 Abundance Scan 1428 (18.154 mln): 28322.D (-) .......... pm/ z 43.00 100.00% 43 __ 57 73 5000 111 95 ---- PTT |TT1 ‘ TETE | I l l l j l 17.80 18.00 18.20 18.40 ,|||,, II 85 J. „ 127 146 201 m/z 57.0.0 72.25% miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #3286: 2-Propanone, 1-(1-methylethoxy)- 43 %

5000 17.80 18.00 18.20 18.40 58 27 .73 m/z 73.0,0 59.76% mmmm l;l....... I.................................................................................... 111111-1.. |.... |.... |.... |.... 1.... 1.... |.... |.... 1.... |.... 1.... 1.... 1. U . ( m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance 4407: 2-Provene ntrie BHacetylt 43 111 —------- 17.80 18.00 18.20 18.40 5000 m/z 111.1,0 47.39%

15 77 52 ' | 94 TT । ■" ‘ । TWTTIOUITT l‘‘“l Thm i' ■ • ■ i ■ ■ ■ ■ । i.|....j...., miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #64228: Pentane, 2,3,4-trimethyl- ------ 1 ■ i ' ' • • i • 43 17.80 18.00 18.20 18.40 71 m/z 29.70% 5000

27 55

m/z-> 15 | TOgu mp 114 'I m [ > 11rp11111111[11111।1111 . । 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 1 PIvtiit 17.80 18.00 18.20 18.40

28322.D GCMS1126.M Wed Feb 06 12:56:08 2002 Page 7

NYC-WTC_000018504

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NYC-WTC_000018504Source: NYC Law Department, mirrored locally

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