GC/MS calibration data for sample 28323, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\l\DATA\DEC2701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 2-Propanone, 1-(1-methylethoxy Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T.

18.16 1.00 ug/1 524396 Acenaphthene-dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone/1- (1-methylethoxy) - 116 C6H12O2 042781-12-4 16 2 2-Propenenitrile, 3-(acetyl oxy)- ill C5H5NO2 014268-54-3 12 3 Cyclohexane, 1,4-dimethyl-2-(2-me th 168 C12H24 054411-17-5 10 4 Cyclohexane, 1,4-dimethyl-2-octadec 364 C26H52 055282-02-5 10 Abundance .4 Scan 1428 (18.157 mln): 28323.D(-) m/ z 43.05 100.00% 43 57 73 111 5000

I 85 95

, 127 146 201 . y ... 17.80 18.00 18.20 18.40 mmmmm 11 rTrt .VI. oh j 1111111 vapaadgos rrpTrrp-rr m/z 57.00 73.31% m/z~> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #3286: 2-Propanone, 1-(1-methylethoxy)- 43 % 5000- PTTgumgTtTuumgr 17.80 18.00 18.20 18.40 27 58 73 m/z 73.00 61.18% . .. .I.... I................................................ ... miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #2407: 2-Propenenitrile, 3-(acetyloxy!- 43 111 —TT'! 1 r "Tt ri ITTm"1trrrlt 17.80 18.00 18.20 18.40 5000 m/z 111.10 51.28% 15 77 ? ........52........ ..... ....................................................... ........... ......... miz-> ' 10 20 30 40 50 60 70 80 90 100 110120 ‘130140150160170180 190 200 210 Abundance #14765: Cyclohexane, 1,4-dimethyl-2-(2-methylpropyl)-, (1.a ■ i ■ • • ■ i ‘ ■ 1 ■ i • ■ ■ ■ i 1

69 1 1 17.80 18.00 18.20 18.40 m/z 69.00 30.56% 55 5000 27 42 97 168 125 | .. ।.... ।j.... (I H . ।. .'I', ।| up* i“‘‘ ... ।. i-.. ।.... ।. ।. .j.... ।... 11... 11.... ।.... . ।.., TuKDTTTTefTTT miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 210 17.80 18.00 18.20 18.40

28323.D GCMS1126.M Wed Feb 06 13:01:51 2002 Page 7

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