NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\DEC2701\28323.D Vial: 63
Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 6 2H-1,4-Benzodiazepin-2-one, 7- Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
17.45 19.93 ug/1 9848310 Naphthalene-d8 15.28
Hit# of 5 ntative ID MW MolForm CAS# Qual
1 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22
2 Silane,/fl,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12
3 l,l,l}/,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 12
4 3-Trimethylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 9
Abundance Scan 1351 (17.450 min): 28323.D (-) m/ z 73.00 100.00%
73
5000
45 L
147
341
429
...... I]........
17.20 17.40 17.60 17.80
96 117 179.207225 251 281 311 L h 367 397
I
0- notk 111 11! Hprf J' I TlT|1 T l 11' 7 m/z 341.00
[ T t 11 1I11 f11 ft 11V1ii |) 1i "I ] : (11 | A 111Ti111111111 11 Q i 34.07%
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440
Abundance #48337: 2H-1,4-Benzodiazepin-2-one, 7-chloro-1 ,3-dihydro-5-
73 341
5000
17.20 17.40 17.60 17.80
45 m/z 147.00 15.35%
91
Tpmg I 116 146 T 227 269 315
,.... ।।.... ।।.... ।.«> > । .1.. ‘‘B——B—B4B8‘5*77**H**
40 60 80 10012014016018020022024026028 0300320340360380400420440
Abundance 448324: Silane, [1,2.3-benzetictriyitrisioxyltisgtmerhyl
I 73
239 17.20 17.40 17.60 17.80 '
5000 342 m/z 342.00 11.35%
45
133 179 211 । 314
.।j....j।।. I.... 1.... I1.... 1H 11!11.1
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440
Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3.3-bis(trimethylsiloxy)t
73 17.20 17.40 17.60 17.80
m/z 325.00 11.02%
147
5000 267
355 429
45 207
m/z->
..... I,.'.... Hpmpa
40 60 80 100120140160180200220240260280300320340360380400420440
[
17.20 17.40 17.60 17.80
28323.D GCMS1126.M Wed Feb 06 13:01:46 2002 Page 6
NYC-WTC_000018530
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