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GC/MS calibration data for sample 28323, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018519–000018545

Folder label: “GCMS X 12/18/01 A 12/30/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 2H-1,4-Benzodiazepin-2-one, 7- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

17.45 19.93 ug/1 9848310 Naphthalene-d8 15.28

Hit# of 5 ntative ID MW MolForm CAS# Qual

1 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 2 Silane,/fl,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12 3 l,l,l}/,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 12 4 3-Trimethylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 9 Abundance Scan 1351 (17.450 min): 28323.D (-) m/ z 73.00 100.00% 73

5000

45 L 147 341

429 ...... I]........ 17.20 17.40 17.60 17.80 96 117 179.207225 251 281 311 L h 367 397 I 0- notk 111 11! Hprf J' I TlT|1 T l 11' 7 m/z 341.00 [ T t 11 1I11 f11 ft 11V1ii |) 1i "I ] : (11 | A 111Ti111111111 11 Q i 34.07% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #48337: 2H-1,4-Benzodiazepin-2-one, 7-chloro-1 ,3-dihydro-5- 73 341

5000 17.20 17.40 17.60 17.80 45 m/z 147.00 15.35% 91 Tpmg I 116 146 T 227 269 315 ,.... ।।.... ।।.... ।.«> > । .1.. ‘‘B——B—B4B8‘5*77**H** 40 60 80 10012014016018020022024026028 0300320340360380400420440 Abundance 448324: Silane, [1,2.3-benzetictriyitrisioxyltisgtmerhyl I 73 239 17.20 17.40 17.60 17.80 ' 5000 342 m/z 342.00 11.35% 45 133 179 211 । 314 .।j....j।।. I.... 1.... I1.... 1H 11!11.1 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3.3-bis(trimethylsiloxy)t 73 17.20 17.40 17.60 17.80 m/z 325.00 11.02% 147 5000 267 355 429 45 207

m/z-> ..... I,.'.... Hpmpa 40 60 80 100120140160180200220240260280300320340360380400420440 [ 17.20 17.40 17.60 17.80

28323.D GCMS1126.M Wed Feb 06 13:01:46 2002 Page 6

NYC-WTC_000018530

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NYC-WTC_000018530Source: NYC Law Department, mirrored locally

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