Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
NYC-WTC_000036614–000036644Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\JAN0802\29466.D Vial: 6 Acq On 8 Jan 2002 5:14 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************************** * * * * * * * ****************** Peak Number 6 2H-1,4-Benzodiazepin-2-one, 7- Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
17.31 30.69 ug/1 14317900 Naphthalene-d8 15.13
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 2 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 16 3 Silane, [1,2, 3-benzenetriyltris(oxy 342 C15H3003Si3 017864-23-2 12 4 Cyclohexasiloxane, dodecamethyl - 444 C12H3606Si6 000540-97-6 8 Abundance Scan 1336 (17.311 min): 29466.D (-) m/ z 73.00 100.00% 73
5000 341 147 17.00 17.20 17.40 17.60 45 , 96 117 . 179 207225 251 281 311 ( 367 397 429 — TTTCT’T’ TIT 1111 rp i Y i TTTTTT i r 11 —TpT TTTgu TTTTTTTTTTTTT m/z 341.00 30.02% m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380400420 440 Abundance #48337: 2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- 73 341
/ 5000 "I 17.00 17.20 17.40 17.60 45 91 m/z 147.00 14.30% 116 146 227 269 3151 1 "]• l pp T’TTTICITTTTT’T m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 440 Abundance #56714: 1.1.1.5,7.7.7-Heptamethyl-3.3-bis(trimethylsiloxy)t 73 100 147 17.00 17.20 17.40 17.60
5000 267 m/z 325.0.0 10.60% 355 429 45 , 207 i ■ . , 1 i"" i" " i" ■ • i ■ ■ • ■ i" "i" T’TuI’UEITEIE-IEEUIIVCTEIETTTTETETTEEE’TETTTTETTTTETETTTETTE ’ITTT m/z--> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 440 Abundance #48324: Silane, [1,2.3-benzenetriyltris(oxy)]tris[trimethyl- 73 17.00 17.20 17.40 17.60 m/z 342.00 1 0.29% 239 5000- 342
45 133
mlz-> 4 I I’ 179 211 TTTTTT i"' ■ I E’EITTTTTTT "314 1 " r'" r " ■ i1H' i 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440 17.00 17.20 17.40 17.60
29466.D GCMS0103.M Wed Jan 09 16:16:23 2002 Page 6
NYC-WTC_000036629
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NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018287
Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
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NYC-WTC_000036491
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
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NYC-WTC_000036492
Fragmented page from a DEP environmental sampling record containing partial text and data fields.
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NYC-WTC_000036494
Laboratory calibration data sheet for GCMS analysis of organic compounds including nitrosamines and chlorobenzenes dated December 13, 2001.
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NYC-WTC_000036498
Laboratory report detailing GCMS calibration analysis for various organic compounds including nitrosamines and chlorobenzenes conducted on December 13, 2001.
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NYC-WTC_000036503
Laboratory report documenting GCMS blank analysis for organic compounds conducted on January 4, 2002, showing results below detection limits.
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