NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30426.D Vial: 23
Acq On : 28 Dec 2001 11:28 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 4 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
17.45 4.48 ug/1 1870660 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25
2 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22
3 Silane, [1,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12
4 3-Trimethylsilyloxystearic acid, tr 444 C24H52O3Si2 000000-00-0 9
Abundance Scan 1352 (17.453 mln): 30426.0 (-) m/z 73.00 100.00%
73
5000
341
147 429
45 17.20 17.40 17.60 17.80
99117 179.207225 251 281 311
m/z 341.00 34.18%
miz-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsitoxy)t
73
147
5000 267 17.20 17.40 17.60 17.80
355 429
45 207 m/z 147.00 14.19%
miz—>
mmmmmmmmmmp
40 60 80 100 120140160180 200 220 240 260 280 300 320 340 360 380 400 420 T‘
Abundance #48337; 2H-1,4-Benzodiazepin-2-onc 7-cnloro-1 3-dihydro-5-
73 341
17.20 17.40 17.60 17.80 1
5000 m/z 324.90 11.38%
45
91
[116 146...... 227. 269...315 . ....... ..
m/z-> 40 60 80 100120140160180200 220 240 260 280 300 320 340 360 380 400 420 T
Abundance। #73587: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethyl- ——
73 239 17.20 17.40 17.60 17.80 '
t m/z 342.00 11.12%
342
5000
45
133
I —8010338117
1111111209—010150111301113010 211.. ’010—30111311T
11 ■ ‘ ‘' I'"' 11
m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 17.20 17.40 17.60 17.80
30426.D GCMS1126.M Wed Jan 02 11:07:52 2002 Page 4
NYC-WTC_000017735
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