Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018519–000018545Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\DEC2701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method.: C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Cyclopentasiloxane, decamethyl Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
14.31 14.05 ug/1 6940960 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual l Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 2 Benzoic acid, 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 38 3 Benzeneethanamine, N-[ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 38 4 N-(TrjTluoroacetyl)-0,0',0''-tris(t 481 Cl9H34F3NO4Si3 000000-00-0 35 Abundance Scan 1009 (14.311 min): 28323.D (-) m/z 73.0,0 100.00% 73
5000 267 355 1.1"* * • I r. . i j . । . j » , । ) । 45 , 1 89 108 133 154 177 193208223 251 14.00 14.20 14.40 14.60 ’ ’I’ i ’V ’*1’* ’TITt* ’1 nfi । n Pi TT+rT । TV i IT1’ ITI j TTI 293308323339 4— m/z 267.00 38.54% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 *’I*11**I***I! 14.00 14.20 14.40 14.60 m/z 355.05 31.82% 191 207 251 323339 r • ‘' i'' ” i “ • • i 1+*****) TTTT 1’2111 1’3 I’T m/z->____ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance 72298: Benzoic oo 2-ittimethylsik tn netiryls 73 267
14.00 14.20 14.40 14.60 5000 m/z 356.05 11.12% 135 175 193 209 233249 ; 282 47 ____L ‘' i ■ ■ " i ■ ■ " i ■ ■ ■ ■ i ■11' I' " 1111111 " 1 ‘11 “ 111 " IF ’ I " 1' 1 ■ “ । । ■ i ■ ■ ■ ■ i • ■ • ■ 1111111 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74573: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 14.00 14.20 14.40 14.60 m/z 268.00 10.22% 5000- 267 44 ... . .. 151 179194299 . 250 ..... 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 miz—> 14.00 14.20 14.40 14.60
28323.D GCMS1126.M Wed Feb 06 13:01:41 2002 Page 5
NYC-WTC_000018529
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NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018287
Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
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NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
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NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
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