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GC/MS calibration data for sample 28323, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018519–000018545

Folder label: “GCMS X 12/18/01 A 12/30/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Azetidine, 1-methyl- Concentration Rank 20

R.T. EstConc Area Relative to ISTD R.T.

12.95 0.69 ug/1 262355 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Azetidine, 1-methyl- 71 C4H9N 004923-79-9 50 2 Nona: , 3,7-dimethyl- 156 C11H24 017302-32-8 50 3 Deca e. 2,6,6-trimethyl- 184 C13H28 062108-24-1 45 4 Pentane, 2,2,3,4-tetramethyl- 128 C9H20 001186-53-4 43 Abundance Scan 861 (12,952 min): 28323.D (-) m/z 57.00 100.00% 57

43 71 5000 85 naospund JIp 99 112 11 r I’I’i . 111111!. i n [ iS itt 141150 207 TTTt 12.60 12.80 13.00 13.20 m/z 71.10 60.02%

MN miz-> 20 30 40 60 50 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 Abundance ' ” ' #246: Azetidine, 1-methyl- 30 42

5000 56 ' 71 12.60 12.80 13.00 13.20 m/z 43.05 57.55%

m/z-> 'Abundancei

5000 'i•“‘ “"i 'I|H >.|I ...| 11.|।....।J...-!....|.... | ....| .... | . > . . | . . . :20 30 40 50 60 70 80 90 100 110120130140150160170180190 200 210

43 57 71 #11601 Nonne, 3.-dimethy:

VWwr 12.60 12.80 13.00 13.20 1 m/z 56.00 51.92%

NA_ 85 127 97 ’*’’’++++*8’1 156 । 11 । i > 111 > > । 11 i । । > i । i 11 1111 i OT—T1—433, miz-> :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance। #19023: Decane, 2,6,6-trimethyl- 57 12.60 12*80 13.00 13.20 ' i/z, 41.05 35.47% 5000 43

m/z~> •I’ I” “I ’ ’ “ I I 85 99 71 1, I . 1 . . . I',I . . . . I . . . . I . 14/ I I . . . .'1'1 . . . I . . I 1. I . . . . 1 . , , , 1 , . . . I . . . . 1 . . . , I . . . . 1 . . . . I . . . , I . . , 20 30 40 50 60 70 80 90 100110120130140150160170 180 190 200 210 W/W * । • •»»। • • • • । •. •. । 12.60 12.80 13.00 13.20 > । । r

28323.D GCMS1126.M Wed Feb 06 13:01:37 2002 Page 4

NYC-WTC_000018528

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NYC-WTC_000018528Source: NYC Law Department, mirrored locally

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