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GC/MS analysis results for sample AD22549, September 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD22549 conducted on September 27, 2001, identifying unknown compounds.

NYC-WTC_000087022–000087043

Folder label: “508 Scan 9/18/01 9/27/01

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Scanned page image, NYC-WTC_000087035
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2601\22549.D Vial: 3 Acq On : 26 Sep 2001 12:17 pm Operator: GALOS Sample : GC/MS unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DATABASE\NBS75K.L Peak Number 6 Azetidine, 1-methyl- Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

29.81 0.46 ng/uL 35285 Chrysene-dl2 33.30

Hit# of 5 Tentative ID MW MolForm CAS# Qual

i>j^etidine, l-meth"l- 71 C4H9N 004923-79-9 5 2 Pentane, 2 -bromo- 150 C5HllBr 000107-81-3 4 3 Pent>me, 2,2- dime?:ly 1 - 100 C7H16 000590-35-2 4 4 Butane\^2-bromo-i: - methyl- 150 C5HllBr 000507-36-8 4 Abundance \ C i.i 2723 (29.807 min): 22549.D (-) m/z 57710 100.00% 5|7 43 71 afiS 85 I ' ' ' ' I ' ' 29.40 29.60 29.80 30.00 30.20 '' I'''' I'''' I'''' I'''' I ' ‘ I '''' I ''' I " ' ' I' I'''' I'''' I'''' I m/z 43.10 75.35% m/z-> 10 20 30 40 50 .1 70 80 90 100 110 120 130 140 150 Abundance 7246: Azetidine, 1-methyl- 3b 42

5000 71 29.40 29.60 29.80 30.00 30.20 m/z 71705 62704% ill 4^ I'''' I'''' I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66675: Pentane, 2-bromo- 43 71 -p-r-n-p- 29.40 29.60 29.80 30.00 30.20 5000 27 m/z 41710 35.90%

'' I''''11'I'I' I '111 107 123 150 ‘ I ' ' ' ' I I '' ' I ' I ' ' ' ' I ' ' ' ‘ I' ' ' ' I ' ' * -rp-i 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance . #1592: Pentane, 2,2-dimethyl- 5|7 29.40 29.60 29.80 30.00 30.20 43 m/z 85.05 35774%

5000 29 85

15 ' I'''' I'''' I'''' I'''' r 10 20 30 40 50 69 70 80 90 100 110 120 130 140 150 . .1 29.40 29.60 29.80 30.00 30.20

22549.D NP072501.M Mon Oct 01 14:40:29 2001 Page 6

NYC-WTC_000087035

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NYC-WTC_000087035Source: NYC Law Department, mirrored locally

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