GCMS Analysis Report for Sample AD26336, Dec 2001

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Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3 001\2633 6.D Vial: 30 Acq On 1 Dec 2001 2:36 pm Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Aziridine, 2,2-dimethyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 5.17 0.85 ng/uL 271471 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Aziridine, 2,2-dimethyl- 71 C4H9N 002658-24-4 28 2 1-Hexene / 84 C6H12 000592-41-6 9 3 1-Hexanol / 102 C6H140 000111-27-3 9 4 1-Pentanol, 4-methyl - 102 C6H140 000626-89-1 9 Abundance Scan 36 (5.169 min): 26336.D (-) m/z 41.10 100.00% 41 56 59

5000

TII >।। . TITTTDTTTT 84 . 444 Trrrrp-rTTT mmmmT 49 71 UN m/z ‘ 5.00 ' ‘ 5.20 56.10 ' 5.40 ' ' 5.60 89.48% mfe-> 5 1C 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 ............................................... ...... Abundance #248: Aziridine, 2,2-dimethyl- 33 56 3942 5000 27 71 5.00 5.20 5.40 5.60 15 m/z 59.05 78.54% TH TPPT mp— m .... 1.111PI,, I.... I... 111.1 mPP mm mm "i"" mlz—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance

5000 #62754: 1-Hexene 41

27 56

5.00 m/z42.00 M 5.20 5.40 78.10% 5.60

AW 84 69

miz-> 5 ..,.... ।....।.।. ‘' I'' " I “ ' +504 I' ‘' I' " ' I'' ‘ I' ‘‘ I ‘ ‘‘ 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63564:1-Hexanol 1 । * 43 55 5.00 5.20 5.40 5.60 m/z. 43.05 69.04% 31 5000 27 69 84 l • •। • ■ ■ ■ । ■ 73 m/z—> Hm 1111 ii 111111 ri y 111 ’II ‘ " I * • * • 1 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 |iiii|iiti|iiil|iiii|iiii .. । .... i frui । TrTr 5.00 5.20 5.40 5.60

26336.D NP112701.M Tue Dec 04 15:07:50 2001 Page 3

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