GCMS analysis results for sample AD28167, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2101\28168.D Vial: 18 Acq On : 22 Dec 2001 10:19 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1-Aziridineethanol Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.15 2036100.00 ng/uL 101805 Acenaphthene-diO 0.00

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Aziridineethanol 87 C4H9NO 001072-52-2 25 2 1-Butanol/ 74 C4H10O 000071-36-3 23 3 Methoxyacetonitrile 71 C3H5NO 001738-36-9 10 4 Cyclobutane 56 C4H8 000287-23-0 9 Abundance Scan 33 (5.148 min): 28168.D (-) m/ z “10 100.00% 41 56 59

5000 71 45 5.00 5.20 5.40 5.60

miz-> ।. mTTT TT mmmm l+ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 r,,,r,"i " i" " r "' r'' ■ i'H' i'' m/z 59.10 77.91% Abundance #754:1-Aziridineethanol 56 42

5000 5.00 5.20 5.40 5.60

A 27 31 m/z 56.10 74.11% 45 i" " i" " i" " r ‘‘I‘ TTPTT Tth..... ..... ..... , p-m-p rTTp-TTTp-TTTp-rTTpTTTpTTTpT mz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62584: 1-Butane! 41 56 AAA5.00 5.40 5.60 5000 m/ z 69.51%

38 110111—010111—1—0000—0—T‘TT"T | I I I I | I I I I |4 4 I I | I ■ I I | I I t I | t I I I | I I I I | 45.531......... miz-__ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #240: Methoxyacetonitrile AA

X 41 5.00 5.20 5.40 5.60 29 m/z 42 .10 52.23% 5000 70 15 26 38 44 54 A i" " r T-rp-mp-rr ..... I' T m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 5.00 5.20 5.40 5.60

28168.D NP112701.M Fri Dec 28 09:58:55 2001 Page 1

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