GCMS analysis results for sample AD27544, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1301\27544.D Vial : 3 Acq On : 13 Dec 2001 12:12 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

• Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclobutane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.20 0.52 ng/uL 200982 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

I Cyclobutane/ 56 C4H8 000287-23-0 9 2 1-Aziridineethanol 87 C4H9NO 001072-52-2 9 3 1- But anol 74 C4H10O 000071-36-3 9 4 Pentane, 2-methyl- 86 C6H14 000107-83-5 9 Abundance Scan 39 (5.197 min): 27544.D (-) m/ z 41..05 100.00% 41 56 59 5000 71 — ————1—0001 TfI— 45 5.00 5.20 5.40 5.60 ।।1.1111 38 - 53/44 ■ r ■ ■ • i ■ r ■ ■ ■ i1 ■ ■' i ■' ■' i' ■ ■ • i' m/ z 59.10 69.20% m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62310: Cyclobutane 41 56

5000- 27 ....................... — 5.00 5.20 5.40 5.60 m/z 43..10 68.25% 3& 49 53 TTTTH 1 ■111 •111" ।1 ■ ■ i ■ • ■ ■ । 1111TTTTT '''' i " 1' i11 " i ।■ ■ ■■। ■ ।' m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #754: 1-Aziridineethanol 56 42 —I 5.00 5.20 5.40 5.60 5000- m/ z 56.10 66.34% i 27 31 li TTTT • i ■ ■ ■ ■ । 45 ■ i • • ■ ■ i ■ — 71 87 • r 1 ■ ’ i' •' ■ i • >'' । ■ • ■ ■ । -' m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62584: 1-Butanol ........... . 41 . 56 5.00 5.20 5.40 5.60 m/z 42.. 10 56.65% 5000-

— .. ,. .. ,-3 4 45+53 c 9 . । । ... । . । ■ । > । । A Wz-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 5.00 5.20 5.40 5.60

27544.D NP112701.M Fri Dec 14 12:53:48 2001 Page 1

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