GCMS analysis results for sample AD26682, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0501\26682.D vial: 2 Acq On 5 Dec 2001 9:41 am Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Cyclobutane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

5.07 0.87 ng/uL 298217 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclobutane 56 C4H8 000287-23-0 16 2 Cyclobutane 56 C4H8 000287-23-0 9 3 Aziridine, l-methyl- 57 C3H7N 001072-44-2 9 4 1-Propene, 2-methyl- 56 C4H8 000115-11-7 9 'Abundance Scan 25 (5.074 min): 26682.D (-) m/z 41.10 100.00% i 41 56 59

5000-

45 71 I > 11 >“l l ... I ■

4.90 5.00 5.10 5.20 5.30 5.40 5.50 N 1 I । । ' । I TTTITrIr r | i i i r । i J 49 53 । — " 11 — | 4 — 67 | ■ 1 i '' ■ ■ i m/z 56.10 87.29%

N m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 'Abundance #62310: Cyclobutane I 411 56

5000- 27 p • • • । " ‘TT’It n11 ‘ I Tur 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 59.10 76.43% piH |> >llr > । i ■ i i । i 38 -i-rTTTT-I-ri-rt-rT+ 49 53 TTrTr‘Tr1rrrrtrt1ri111 m/z--> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #80: Cyclobutanc 41 | I I I I j inip.. . | I . I > I ■' i' ■' ■ i ■' 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 - 56 m/z 42.10 65.22%

JA 27

37 49 53 T‘U1T0-ETIIII 111 < I I . I . .. f-l30 I , J . , I , TTTuupnIwuu,BumPum] m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #86: Aziridine, 1-methyl- I 4b 43.00 49.48% 5000 - 57

15

m/z-> 5 10 15 .... 4120...... 20 25 30 35 40 54 TTp-rrrpi TIIT 45 50 55 1' I' ' '' I '''' I ' '' ' I ' '' ■ I 60 65 70 75 80 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26682.D NP112701.M Fri Dec 07 13:13:14 2001 Page 2

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