GCMS analysis results for sample AD26321, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26321.D Vial: 31 Acq On : 1 Dec 2001 3:30 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclobutane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 5.22 0.47 ng/uL 142071 1,4-Dichlorobenzene-d4 11.88 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 Cyclobut he 56 C4H8 000287-23-0 12 2 1-But ano1 , 2-methyl-, (S) - 88 C5H120 001565-80-6 9 3 1-Aziridineethanol 87 C4H9NO 001072-52-2 9 4 1-Butanol 74 C4H1O0 000071-36-3 9 Abundance f Scan 41 (5.217 min): 26321 .D (-) m/z 41 .10 100.00% 41

_N 56 59

5000

71 5.00 5.20 5.40 5.60 TTmnagt 38 45 5053 67 TTTT 1 i ■1 “ i'1 “ i ' • i “ 1' i ■11 • i1 ■ ■ ■ i “ “ i " m/z 59.10 71.55% m/z—> 15 20253035404550 55 6065 70 75 80859095 Abundance #62310: Cyclobutane 41 56

5000 27 - 5.00 5.20 5.40 5.60 m/z 56-05 66.83% TTppnutt TITTHHT — 49 H 53 1 ‘ ‘ I ‘ ‘ ‘ I ‘ ‘‘ I ‘1' ■ I ‘“ I " ' ■ I" ’ ‘ I ‘1111' • 38

AN _ m/z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62950: 1-Butanol, 2-methyl-, (S)- 41 57 -AA4 5.00 5.20 5.40 5.60 5000 31 m/z 43.10 63.68% 27 70

miz-> Abundance L. Th 53 — HTTTTT 37 ■ i “ •' i 15 20 25 30 35 40 45 50 55 60 65 #754:1-Aziridineethanol ‘I , rn^ " .-rm-m-p-. . > I "‘‘I1TT 70 75 80 85 90 95 JW 42 56 ■ ■ 5.00 I ' ' ‘ ‘ l 5.20 ‘ I 5.40 5.60 m/z 42 00 58.02%

_N 5000

27 31 15 - I. 71 87 "TTTT ’ I “ ' ‘ I ' ——— T-r-f i i ■ ■ TTT T II —AAAA m/z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 5.00 5.20 5.40 5.60

26321.D NP112701.M Tue Dec 04 10:13:28 2001 Page 2

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