GCMS analysis results for sample AD26321, Dec 2001

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Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3001\26321.D Vial: 31 Acq On 1 Dec 2001 3:30 pm Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Ethane, 1,1-diethoxy­ Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 7.18 0.40 ng/uL 120579 1,4-Dichlorobenzene-d4 11.88 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethane ,/1,1 - diethoxy- 118 C6H14O2 000105-57-7 39 2 2,3- Butanediol 90 C4H10O2 000513-85-9 33 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 Ethane, 1,1-diethoxy- 118 C6H14O2 000105-57-7 9 Abundance Scan 255 (7.180 min): 26321 .D (-) m/z 45.10 100.00% 45

5000

vfz-> mmmmm 61 73

+H m 1 . | J.'1.., m mpe mpmpm mem 207 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 L 680 m/z 7.00 43.00 । . । ... . । 7.20 7.40 70.87% । 7.60 j

Abundance #64431: Ethane, 1,1-diethoxy- 45

5000 73 ) W, —TI—I—uuTuuetpeunrt 29 680 7.00 7.20 7.40 7.60 103 m/z 61.00 32.66% ■■I ii > > 1111’qk ■ >ii il'i'ii 11 61 1 rr1" 11 mmooon— । ..j।।।11 n ■ 11 >> । mlz—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #917:2,3-Butanediol 45 • i • ■ • ■ I 11 1 1 r* 1 11 11 • * ‘ i ■ • 680 7.00 7.20 7.40 7.60 5000 m/z 73.05 32.46% 29 9 1 mll57 I" “I" “I1 75 90 Ippr ——CIEECIIegr nfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #292: N-Ethylformamide ‘ I ‘ ‘ • I ’ ‘ ' I ‘ ‘ ‘ ■ I ‘ ‘ ' I ‘ 1 33 680 7.00 7.20 7.40 7.60 73 m/z 44.00 16.84% 5000 44 58

15 bwyM/yv 111 m !111 ml miz—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 6.80 7.00 7.20 7.40 ■ i ■ ■ 7.60

26321.D NP112701.M Tue Dec 04 10:13:29 2001 Page 3

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