GCMS results log, sample AD26983, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26983.D Vial: 25 Acq On 7 Dec 2001 7:59 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins . Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 1-Butanol Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

5.15 0.41 ng/uL 146795 1,4-Dichlorobenzene-d4 11.89

Hit# Of 5 entative ID MW MolForm CAS# Qual

1 1-Butanol/ 74 C4H10O 000071-36-3 25 2 Cyclobutane 56 C4H8 000287-23-0 9 3 1-Aziridineethanol 87 C4H9NO 001072-52-2 9 4 1-Butanol 74 C4H10O 000071-36-3 9 Abundance Scan 33 (5.147 min): 26983.D (-) m/z 41.05 “100.00% 41

AN . 56 59

5000

45 71 5.00 5.20 5.40 5.60 | — I m/z-> 15 3813 ,I " " i " " i1 ■ ■ ■ i " ■ ■ r ' 20 25 30 35 40 .1.. 5051155 60 65 70 75 80 85 90 95 45 + m/z 56. 10 75.01%

AN Abundance #62584: 1-Butanol 41 56

5000 —iri T । । । । । । r TmfrTr 5.00 5.20 5.40 5.60 m/ z 59. 10 73.31% 45 53 I : - 111111111 - 111111111111 ■ 11111 TTTTTTT m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62310: Cyclobutane 41 56 A 5.00 5.20 5.40 5.60 27 m/z 43.— 10 70.56%

_N, 5000

38 49 53 ■ ■ ■ ■ i ■ ■' ■ i ‘ ' i'' ■ ■ r ' •' i' TTPTTTTTTTTTTTTTT)*W))WDTTTTIWWIIPPUTTT m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #754: 1-Aziridineethanol TEGrndt I I I T—TdT 56 5.00 5.20 5.40 5.60 42 m/ z 42 . .10 61.98% 5000

m/z-> 27 31 H.... — ----- ■ ।11 ■ ■ i1।। ■ 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 15 AN 26983.D NP112701.M Tue Dec 11 14:49:35 2001 Page 2

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