GCMS analysis results for sample AD27548, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC13O1\27548 .D Vial: 7 Acq On : 13 Dec 2001 3:50 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/.TCLP calibration table Library . : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1-Butanol Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

5.20 0.46 ng/uL 144058 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanol 74 C4H10O 000071-36-3 37 2 l-Butanol 74 C4H10O 000071-36-3 17 3 Cyclobutane 56 C4H8 000287-23-0 9 4 3-Pentanol 88 C5H120 000584-02-1 9 Abundance Scan 39 (5.200 min): 27548.D (-) m/z 41.10 100.00% 41 43 56 59

5000 39 i — ' i ' -AA i '

m/z-> 15 Abundance 20 25 30 35 — 40 +45...50m55 + 60 65 70 #62584: 1 -Butanol l ■ i ■ ■ ■ • i ■

75 80 5.00 m/ z 5.20 56.10 5.40 5.60 71.63%

41 56 43

5000- -------A 5.00 5.20 5.40 5.60 39 m/ z 43.10 70.75% ............. 37 11 ■ । ■ ■' ■ । ■ ■ ■ ■ ।1' ■ • । ■ ■111 145 . 53 ' 1 . ... TT 11111111111111 ■ ■ । ' i ■ ■ ■ ■ । • m/z-> 15 20 25 30 35 40 45 50 :55 60 65 70 75 80 Abundance #62580: 1-Butanol 3,1 56 27 41 43 । i I 5.00 5.20 a5.40 .. 444 5.60 I i 5000 I । m/z 59.05 69.03% i 33 38 45 1 i I l TT-rT-T-TT-p-r-r-r-pnrr-r-p-T-r-ry-r-rT-r-p-TTT-pn-Tn-p-T-r-r-n-^^ 73 ■ ' i ' ' 1 ' i ' ' ' 1 i m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #62310: Cyclobutane ..... — P -P 41 5.00 5.20 5.40 5.60 56 m/z 42.05 51.73% 5000 27

39

m/z~> 15 25 ' 1 1 1 1 1 1 r1 20 25 ■ ' i ' ' ' ' i 30 35; 37 40 45 49 53 I ■ > l ■ ■ ■ > I 1 1 1 + 1 • ■ । ■ ■ ■ ■ । 50 55 60 65 ■ i ■ ■ ■ ■ । • ■ ■ ■ । •

70 75 80 4-A 5.00 5.20 5.40 5.60

27548 .D NP112701.M Fri Dec 14 12:56:03 2001 Page 1

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