GCMS calibration data for TCLP analysis dated December 7, 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C: \HPCHEM\ 1 \DATA\DEC0 7 01 \LB. D Vial: 2 Acq On 7 Dec 2001 7:01 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Butanol Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 5.09 1.76 ng/uL 545324 1,4-Dichlorobenzene-d4 11.88 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanol 74 C4H10O 000071-36-3 47 2 1-Pentanol, 4-methyl- 102 C6H140 000626-89-1 33 3 1-Hexene 84 C6H12 000592-41-6 33 4 Pentane, 2,3-dimethyl - 100 C7H16 000565-59-3 32 Abundance Scan 27 (5.087 min): LB.D (-) m/z 41 05 100.00% 41 56

5000

45 71 4.90 5.00 5.10 5.20 5.30 5.40 5.50 ‘ 1091111111111 —374 +51 + | 100 ‘1—011—0—0000290 rrrrn-r, 10111 m/z 56.10 77.68%

A_ tnfz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #62584:1-Butanol 41 56

5000 TTT 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 59.10 72.47% 45 37 n |. u . 11. n !.... j.. I H *Tmmu] miz—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63578: 1-Pentanol, 4-methyl- 56 41 i “ " i ■ • TIMTTIT TIOm i i-r^r 69 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 m/z 42.05 69.79%

mfz~> Abundance 45 60 84 TTT1, TT—n——uTT]mmmpmpm] 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 41 #62753:1-Hexene 56 N 1’1 1’11 TT‘01‘71‘TTT—ur 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z4. 43.10 62.05%

m/z—> 5000

— 27

,| f. ... 52, . - 69

T 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 1 4.90 ....... i■•■■i 84

....... TUITrTTT 5.00 5.10 5.20 5.30 5.40 5.50 ... 7 LB.D NP112701.M Thu Dec 13 11:28:24 2001 Page 2

NYC-WTC_000031672