GCMS calibration data for TCLP analysis dated December 7, 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC0701\LB.D vial: 2 Acq On 7 Dec 2001 7:01 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.0G MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Pentane, 2,3-dimethyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 5.15 4.53 ng/uL 1405930 1,4-Dichlorobenzene-d4 11.88 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentane, 2,3-dimethyl- 100 C7H16 000565-59-3 46 2 Pentane, 2,3-dimethyl- 100 C7H16 000565-59-3 43 3 Pentane 2,3 -dimethyl - 100 C7H16 000565-59-3 37 4 1-Pentene, 4-methyl- ______ 84 C6H12 000691-37-2 25 Abundance Scan 34 (5.151 min): LB.D (-) m/z 4 .10 100.00% 41 56

5000

----- +40 5141 1 71 100 TIT TT TIT । i । । _N m/z 5.00 5.20 5 .10 1 i ' TTI i • 5.40 5.60 75.31% m/z-> 10 20 30 50 60 70 80 90 100 110 Abundance #63432: Pentane, 2,3-dimethyl- 56

5000 27 43

71 m/z 5.00 N . 5.20 59.10 5.40 72.83% 5.60 , 85 miz-> • * i • ' > * i * * ■ * । ' • • • i 10 20 30 40 50 — 60 l70..80 — 90. - 100 1 I 1 1 1 1 I 1 100 110 Abundance #63429: Pentane, 2.3-dimethyl- 43 56

5.00 5.20 5.40 5.60 29

7 5000 m/z 43.10 69.77% 71

15 85 100 1 1 I 1 ■ 1 • i ■ ■ ■ ■ i ■ ■ • • i ■ ■ • • i ■ ■ ■ ■ i ■ ■ ■ ■ i 1 1 1 ' i ' ■ i ■ TTn i 1 1 1 1 1 1 miz—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63431: Pentene, 2,3-dimethyl- 43 56 5.00 5.20 5.40 5.60 62.07% 5000

m/z—> 10 15 i 29

■ ■ i ■ ■ • ■ i ■ ■ ‘ ■ i ■ • • ■ I 20 30 40 ‘ * 1 ‘ * 50 60 71

1 85, +100— 70 80 90 100 110 A • ■ 5.00 i ■ 1 ■ • 5.20 i • ‘ • 5.40 i ■ ■ ■ ‘ 5.60 t *

LB.D NP112701.M Thu Dec 13 11:28:26 2001 Page 3

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