GCMS calibration data for TCLP analysis dated December 7, 2001

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Library Search Compound Report Data File C: \HPCHEM\ 1 \DATA\DEC0 7 01 \LB. D Vial: 2 Acq On 7 Dec 2001 7:01 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Hydrogen azide Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

5.00 1.73 ng/uL 536306 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrogen azide 43 HN3 007782-79-8 4 2 Acetic acid, anhydride 102 C4H6O3 000108-24-7 2 3 Acetic acid, anhydride 102 C4H603 000108-24-7 2 4 4-Penten-2-one, 3-methyl-______ __ 98 C6H10O 000758-87-2 1 Abundance Scan 17 (4.995 min): LB.D (-) m/z , 43.00 100.00% * 43

5000 A p k I j ( 4 , । । j , » । , । iTJYpr 4.90 5.00 5.10 5.20 5.30 5.40

JL ....... ... 36 । [. —5560 ..... ... .. 98... 5.98% miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #33: Hydrogen azide 43

5000 15 p-rTT-p-rT-rp-TT-i ITTT001 4.90 5.00 5.10 5.20 5.30 5.40 29 44.00 2.72%

miz-> 5"10 15 20 25 30 35 40 45 50 55 60 85 70 75 80 85 90 95100105 Abundance #1680; Acetic acid, anhydride 43 1r/8/2/12/22/90//n/21/8/48018,6/.8.8,

A 4.90 5.00 5.10 5.20 5.30 5.40 5000 m/z 41.05 2.19%

- m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63470: Acetic acid, anhydride —TTpmpm 43 4.90 5.00 5.10 5.20 5.30 5.40 m/z. 83.05 1.57% 5000

15 J 29 1, 60 87 10331187 ‘T., T’T,, > 10—————]— P IAA IO m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 4.90 5.00 5.10 5.20 5.30 5.40

LB.D NP112701.M Thu Dec 13 11:28:21 2001 Page 1

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