GCMS analysis sample AD26537, non-target compounds, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 701\26537.D Vial: 4 Acq On 7 Dec 2001 8:51 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Hydrogen azide Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

4.98 2.16 ng/uL 575656 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrogen azide 43 HN3 007782-79-8 4 2 Acetic acid, anhydride 102 C4H603 000108-24-7 2 3 Acetic acid, anhydride 102 C4H603 000108-24-7 1 4 Acetic .cid, 2-propenyl ester 100 C5H8O2 000591-87-7 1 Abundance Scan 15 (4.980 min): 26537.D (-) m/z 43.00 100.00% 4

5000

4.90 5.00 5.10 5.20 5.30 5.40 36 40t , 60 87

A. ’ 11 • i “ ■' i “ “ i “ “ i ‘ ■ • • i “1 ‘ i “ ■ ■ i11 11" “ I" “ I"1' l'1'" 1111' 111" 11 “111"111"11 “ “ 11 m/z 42.00 5.68% mlz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #33: Hydrogen azide 43

5000 15 4.90 5.00 5.10 5.20 5.30 5.40 29 m/z, 44.00 2.92% ■ । •1 " i." ‘ m ***** mz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1680: Acetic acid, anhydride 43

4.90 5.00 5.10 5.20 5.30 5.40 5000 m/z 45.00 1.07%

.......... 29..... ; 60 . 1 .... 1.... 1. I . I I.... I... 11.... 1I I I IljH ... t|111 I | I | | | , 1111! 11 87 miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63470: Acetic acid, anhydride 43 4.90 5.00 5.10 sib 5.30 5.40 m/z 41.00 0.70% 5000 -

15 , 29 1 . 60 87 11—801100000701—0011000—00031000—1- miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 4.90 5.00 5.10 5.20 5.30 5.40"

26537.D NP112701.M Thu Dec 13 11:27:08 2001 Page 1

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