GCMS analysis results for sample AD27550, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC13O1\2755O.D Vial: 9 Acq On 13 Dec 2001 5:39 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 1-Butanol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.20 0.47 ng/uL 189844 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanol 74 C4H10O 000071-36-3 37 2 Cyclobutane 56 C4H8 000287-23-0 9 3 1-Aziridineethanol 87 C4H9NO 001072-52-2 9 4 1-Pentanol, 4-methyl- 102 C6H140 000626-89-1 9 Abundance Scan 39 (5.198 min): 27550.D (-) m/z 41,. 10 100.00% 41 56 59

5000 71 — ——— j 45 5.00 5.20 5.40 5.60

m/z-> .1.... 534 IIITTtIrrtrot 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ■i•■ ■• i•• ■ • । ■ ■ ■ ■ ।■•■ •। ■ m/z 43.. 10 73.21% Abundance #62584: 1-Butanol 41 56

5000 —II r 5.00 5.20 5.40 5.60 m/z 56,. 10 70.78% , 344 45। I.........cT TmmTTTTTTTT m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62310: Cyclobutane 41 56 —MA , 5.00 5.20 5.40 5.60 5000- 27 m/z 59,. 05 68.62%

38 49 53 RTuummummumPmmm]] m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #754:1-Aziridineethanol 56 5.00 5.20 5.40 5.60 42 m/z 42,. 10 60.93% 5000

27 31 15 - L......... 71................ 87.......... 4—0 4 , TA —A l■ • •• i > ■ ' 111 ‘' 11' •' 1' "'I' 11' i " '' TTTTTTTT’1’uur 111111111111111111 m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 5.00 5.20 5.40 5.60

27550.D NP112701.M Fri Dec 14 12:57:21 2001 Page 1

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