GCMS analysis results for sample AD27545, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1301\27545.D Vial: 4 Acq On : 13 Dec 2001 1:07 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C: \DATABASE\NBS75K . L ********************************************************************* Peak Number 1 1-Butanol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.19 0.46 ng/uL 188577 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanol/ 74 C4H10O 000071-36-3 25 2 1-Aziridineethanol 87 C4H9NO 001072-52-2 9 3 Pentane/ 2-methyl- 86 C6H14 000107-83-5 9 4 Aziridine, 1-methyl-_____________ 57 C3H7N 001072-44-2 7 Abundance / Scan 38 (5.194 min): 27545. D (-) m/z 41 ,.10 100.00% / 41 56 59

5000 71 —_ II_ ----- 45 5.00 5.20 5.40 5.60

miz-> I'1’1I' 51 67 TIT । n » rpn fi p i i t । l tP‘0—1TTTTTTT 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 I’’ m/z ‘ 59.10 78.68% Abundance #62584: 1-Butanol 41 56

5000 1.............. Pr 5.00 5.20 5.40 5.60 m/z 43.10 76.59% 45 38 453 rTr’r’d’t" I " 111111 ‘ 11 m/z->5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #754: 1-Aziridineethanol 56 42 5.00 5.20 5.40 5.60 5000 m/ z 56.10 75.88%

27 31 45 71 .I ll i 87 I ' 1 ” ' I"’ 11111" TIT i1" ‘ i I "1 ’ i r ■ ■' i 11 ■ " ■ i' ITTTT T’T m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #733: Pentane, 2-methyl- IT 4b 5.00 5.20 5.40 5.60 m/ z 42.10 56.81% 5000 27 71 39 15 57

m/z-> 5 10 111111 I •' " I .... 53+4...... 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Ti‘ 86 Th...... TIT AA ----- 1 ' 5.00 5.20 — -4-AA 5.40 5.60

27545.D NP112701.M Fri Dec 14 12:54:28 2001 Page 1

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