GCMS analysis results for sample AD26252, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report .Data File C:\HPCHEM\1\DATA\NOV3001\26253 .D Vial: 32 Acq On 1 Dec 2001 4:25 pm Operator: GALOS Sample gc/ms unknown 11/3 +26319 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Butanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 5.19 0.44 ng/uL 143771 1,4-Dichlorobenzene-d4 11.88 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanol 74 C4H1O0 000071-36-3 17 2 Aziridine, l-methyl- 57 C3H7N 001072-44-2 5 3 2-Butene, (E) - 56 C4H8 000624-64-6 4 4 2-Butene 56 C4H8 000107-01-7 4 Abundance Scan 38 (5.187 min): 26253.D (-) m/z 41.05 100.00% 4 56 59

5000 71 । । । 1 . . 45 5.00 5.20 5.40 5.60

mz-> m '1111111" 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 49 I ‘ ‘ ‘ ‘ I ''' ‘ I ■' 111' ’ I m/z 56.10 72.53% Abundance #62584:1-Butanol

5000 41 56

JN _ m/z 5.00 5.20 59.00 5.40 5.60 67.31% 45 ----------- 53 I ‘ • I • ‘ I * I ‘ • I • I ‘ T-p-T ‘11 ‘“ I

miz-> 5 10 15 20 25 30 35 40 50 55 60 65 70 75 80 Abundance #86: Aziridine, 1-methyl- 42 ‘ ■ I • • • ■ l • • ■ • ' • ‘ • l ■ 1 5.00 5.20 5.40 5.60 m/z 43.10 64.84%

JW 5000 57

15 27 2 miz-> ...... Ld 54 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #62302: 2-Butene, (E)- 41 5.00 5.20 5.40 5.60 m/z 42.05 51.21% 56

UN 5000- 27

—30— —1149.......52,1 -P44A44,4 mfz~> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 5.00 5.20 5.40 5.60

26253.D NP112701.M Tue Dec 04 10:11:23 2001 Page 2

NYC-WTC_000031245