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GCMS analysis results for sample AD27550, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AD27550 conducted on December 18, 2001.

NYC-WTC_000033505–000033520

Folder label: “GCMS X 11/15/01 A 12/13/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC13O1\2755O. D Vial: 9 Acq On 13 Dec 2001 5:39 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C: \DATABASE\NBS75K. L

Peak Number 2 2-Hexanone Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.56 0.74 ng/uL 302815 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 91 2 2-Hexanone 100 C6H120 000591-78-6 91 3 2-Hexanone 100 C6H120 000591-78-6 91 4 2-Hexanone 100 C6H120 000591-78-6 90 Abundance Scan 188 (6.564 min): 27550.D (-) m/z 43.10 100.00% 43 58 5000

100

m/z--> m .. 50.4 - TT’T’OTTTTT 391 — 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 71 85 i1 ■'11 I" “ I 6.20 m/ z 6.40 58.10 6.60 6.80 56.37% 7.00

Abundance #1556: 2-Hexanone 43

5000 - 58 ■TI ■ 6.20 6.40 L 6.60 6.80 7.00 m/z 57.10 16.76% 27 39 71 85 100

m/z-> 1 •prrrrn-rrrp-i-i-i T 20 25 — ............... I' fT 30 35 40 45 50 55 60 — m 65 70 75 80 85 90 95 100 105 " I' ■ ‘' I

Abundance 43 #63385:2-Hexanone

6.20 A. 6.40 6.60 6.80 7.00 5000- 58 m/z 41.05 16.39% I 29

MMW I 39 71 100 I 8,5 IWIB—HUUTTp ’ 1 TTT I" " I •''11'' • ‘ I " ‘ • I TV I ’' " I' m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63384:2-Hexanone 43 6.20 6.40 6.60 680 7.00 m/z 100 .05 9.49% 5000 58 29 39

m/z-> TTThr 20 25 m I 71 85 190 11 " " I T TTT "111' 11" " I" " I'' " I" " I' ‘' ■ I ■" ' I" ‘' I' m I 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ........6.40— 46.20 \ 1........................ ,

6.60 6.80 7.00

27550.D NP112701.M Fri Dec 14 12:57:23 2001 Page 2

NYC-WTC_000033514

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NYC-WTC_000033514Source: NYC Law Department, mirrored locally

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