GCMS analysis results for sample AD27765, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC19O1\27765. D Vial : 8 Acq On : 20 Dec 2001 2:18 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 3-Hexanone Concentration Rank 5

R.T. EstConc Area Relative, to ISTD R.T.

6.45 2.67 ng/uL 599309 1,4-Dichlorobenzene-d4 11.87

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Hexanone 100 C6H120 000589-38-8 90 3 3-Hexanone 100 C6H120 000589-38-8 90 4 3-Hexanone 100 C6H120 000589-38-8 64 Abundance Scan 175 (6.446 min): 27765.D (-) m/z 57.10 100.00% 43 57 71 5000 /_/ 100 39 "CKUETDTTDIUT 6.00 6.20 6.40 6.60 6.80

miz-> 53. 4+Hpmp 84 Tp m/Z 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 —mmmmmp 43.10 99.89% Abundance #1528: 3-Hexanone 43 57

5000 29 71 JA 6.00 6.20 6.40 6.60 6.80 100 m/ z 71.05 52.59% TPTTTTTTTT+ TTTTTTTTTTTT 85 '' I'" ' I *' TPTTTTTI F miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63357:3-Hexanone 43 57 —14 . । TTTT r f . । . । । r 29 6.00 6.20 6.40 6.60 6.80 5000 71 m/z 41.10 29 80% 100 __________ .________ 85 i" " r ’' ■ i1 ’'' i I' " ' I .* I ■ • •' I" " i" " I ’ ■' * i ■ • i ‘ ‘11 1 " 1 ‘ rrrrrp-rrrp m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 V Abundance #63358:3-Hexanone 43 6.00 6.20 6.40 6.60 6.80 57 m/z 100.15 28.41% 71 5000

m/z-> mmmmm 11" " r1"111 +........ IT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 TTUTTt 85 I"'•I 100

i""r ... M I ' 1 1 ' I ' ' ' ' I ' ' ‘ ■ n ' ' 6.00 6.20 6.40 6.60 6.80

27765.D NP112701.M Thu Dec 20 11:44:40 2001 Page 5

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