GCMS analysis results for sample AD27625, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC19O1\27625.D Vial: 15 Acq On : 20 Dec 2001 10:39 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Hexanone Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.48 0.92 ng/uL 264992 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Hexanone 100 C6H120 000589-38-8 91 3 3 - Hexanone 100 C6H120 000589-38-8 91 4 3-Hexanone 100 C6H120 000589-38-8 72 Abundance Scan 179 (6.480 min): 27625.D (-) m/z 43.10 100.00% 43 57

71 5000 100 11" 6.20 6.40 6.60 6.80

m/z-> ' ■' r 20 TTTTTT 314 + TTTTTT TTTIIT 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 +85 r m/ z 57.10 89.01% Abundance #63358: 3-Hexanone 413 57 -

71 5000 6.20 6.40 6.60 6.80 100 m/z 71.05 50.20% 85 Hi TTTTTTTTTTTTTTTTTTTT r m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528: 3-Hexanone 43 57 ----- - 6.20 6.40 6.60 6.80 29 71 5000 m/z 100.05 29.69% 100 i 85 “■rp-m-p-rrr-.-rrrymTpT 11"'11" 1' 1111' 1"1' i11" I''1' i ’'1' 11''111111111' ’ I'1'' i11 ■ ■ i11'11 > m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63357:3-Hexanone -1-4 i\______ ' ' I ' ' ' ' I ■ > ■ ■ i • • 43 6.20 6.40 6.60 6.80 57 m/z 41.10 “ 26.45% 29

NA 5000 - 71

100

miz- rr "' r ■ i ■' ■' p1" 11 ’ 1 + 1 i TT TTTTTTTTT’ i ' r "' r " ’ i 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 " i ■' " r ■ " " " r ■'' " " i" ■ ■ r 6.20 6.40 6.60 6.80

27625.D NP112701.M Thu Dec 20 11:40:23 2001 Page 1

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